Abbasian Vahid, Akhlaghi Ehsan A, Charsooghi Mohammad A, Bazzar Maasoomeh, Moradi Ali-Reza
Department of Physics, Institute for Advanced Studies in Basic Sciences, PO Box 45195-1159, Zanjan, Iran.
Department of Physics, Institute for Advanced Studies in Basic Sciences, PO Box 45195-1159, Zanjan, Iran; Optics Research Center, Institute for Advanced Studies in Basic Sciences, PO Box 45137-66731, Zanjan, Iran.
Ultramicroscopy. 2018 Feb;185:72-80. doi: 10.1016/j.ultramic.2017.11.013. Epub 2017 Nov 28.
The aim of this paper is to introduce digital holographic microscopy (DHM) as a non-contact, inexpensive, and non-abrasive method for 3D surface characterization of polymeric nanocomposites. A common-path and vibration-immune Mirau system with a microsphere-assisted arrangement is utilized to increase the lateral resolution of the images. The characterization is performed through the measurement of roughness parameters of the surfaces, which are derived from the recorded holograms. Pure poly(triazole-amide-imide) (PTAI) and PTAI nanocomposite reinforeced with surface modified TiO nanoparticles (MN-TiO) are used and compared. The experimental results show the potential of the presented method to serve as an alternative for expensive surface measurement devices such as stylus profiler and atomic force microscope (AFM) for polymeric surface characterization.
本文旨在介绍数字全息显微镜(DHM),它是一种用于聚合物纳米复合材料三维表面表征的非接触、低成本且无损伤的方法。采用带有微球辅助装置的共光路且抗振动的Mirau系统来提高图像的横向分辨率。通过测量从记录的全息图中得出的表面粗糙度参数来进行表征。使用了纯聚(三唑 - 酰胺 - 酰亚胺)(PTAI)和用表面改性的TiO纳米颗粒(MN - TiO)增强的PTAI纳米复合材料并进行比较。实验结果表明,所提出的方法有潜力作为诸如触针轮廓仪和原子力显微镜(AFM)等昂贵表面测量设备的替代方法,用于聚合物表面表征。