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快速固化非热压罐复合材料的固化周期优化

Cure Cycle Optimization of Rapidly Cured Out-Of-Autoclave Composites.

作者信息

Dong Anqi, Zhao Yan, Zhao Xinqing, Yu Qiyong

机构信息

School of Materials Science and Engineering, Beihang University, Beijing 100191, China.

出版信息

Materials (Basel). 2018 Mar 13;11(3):421. doi: 10.3390/ma11030421.

Abstract

Out-of-autoclave prepreg typically needs a long cure cycle to guarantee good properties as the result of low processing pressure applied. It is essential to reduce the manufacturing time, achieve real cost reduction, and take full advantage of out-of-autoclave process. The focus of this paper is to reduce the cure cycle time and production cost while maintaining high laminate quality. A rapidly cured out-of-autoclave resin and relative prepreg were independently developed. To determine a suitable rapid cure procedure for the developed prepreg, the effect of heating rate, initial cure temperature, dwelling time, and post-cure time on the final laminate quality were evaluated and the factors were then optimized. As a result, a rapid cure procedure was determined. The results showed that the resin infiltration could be completed at the end of the initial cure stage and no obvious void could be seen in the laminate at this time. The laminate could achieve good internal quality using the optimized cure procedure. The mechanical test results showed that the laminates had a fiber volume fraction of 59-60% with a final glass transition temperature of 205 °C and excellent mechanical strength especially the flexural properties.

摘要

非热压罐预浸料由于施加的加工压力较低,通常需要较长的固化周期以确保良好的性能。减少制造时间、实现真正的成本降低并充分利用非热压罐工艺至关重要。本文的重点是在保持高层压板质量的同时减少固化周期时间和生产成本。独立开发了一种快速固化的非热压罐树脂及相关预浸料。为确定所开发预浸料的合适快速固化工艺,评估了加热速率、初始固化温度、保温时间和后固化时间对最终层压板质量的影响,然后对这些因素进行了优化。结果确定了一种快速固化工艺。结果表明,在初始固化阶段结束时树脂浸润可以完成,此时层压板中未见明显孔隙。使用优化后的固化工艺,层压板可获得良好的内部质量。力学测试结果表明,层压板的纤维体积分数为59 - 60%,最终玻璃化转变温度为205℃,具有优异的力学强度,尤其是弯曲性能。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/fae1/5873000/331343839f03/materials-11-00421-g001.jpg

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