Xu Yichen, Unkovskiy Alexey, Klaue Felix, Rupp Frank, Geis-Gerstorfer Juergen, Spintzyk Sebastian
Section Medical Materials Science & Technology, University Hospital Tuebingen, 72076 Tuebingen, Germany.
Department of Prosthodontics at the Centre of Dentistry, Oral Medicine, and Maxillofacial Surgery with Dental School, University Hospital Tuebingen, 72076 Tuebingen, Germany.
Materials (Basel). 2018 Oct 7;11(10):1905. doi: 10.3390/ma11101905.
Computer-aided design (CAD) and additive manufacturing (AM) have shown promise in facilitating the fabrication of custom trays. Due to the clinical requirements, custom tray materials should achieve good bonding to the impression/adhesive systems. This study evaluated the retention of three fused deposition modeling (FDM) custom tray materials to a silicone impression/adhesive system before and after gritblasting (GB) by peel-off test. CAD-designed experimental test blocks were printed by FDM using acrylonitrile butadiene styrene (ABS), polyethylene terephthalate glycol copolyester (PETG), and high impact polystyrene (HIPS), and the reference test blocks were made of a conventional light-curing resin (n = 11). Before and after GB, the surface topography of all tray materials was analysed, and the maximum strength of the test block peeled off from a silicone impression/adhesive system was measured. After GB, the arithmetic mean height (Sa) and the valley fluid retention index (Svi) of the four material groups declined ( < 0.05). The peel-off strength of each of the four material groups significantly decreased by GB ( < 0.05), but no statistical difference could be found among them before or after GB. In all peel-off tests, adhesive failure occurred at the adhesive-impression material interface. The results indicated ABS, HIPS, and PETG could provide sufficient adhesion to the adhesive as the conventional light-curing resin, and GB could reduce the roughness generated by FDM and weaken the bonding between the adhesive and the silicone impression.
计算机辅助设计(CAD)和增材制造(AM)在促进定制托盘的制作方面已显示出前景。由于临床需求,定制托盘材料应与印模/粘结系统实现良好粘结。本研究通过剥离试验评估了三种熔融沉积建模(FDM)定制托盘材料在喷砂处理(GB)前后与硅橡胶印模/粘结系统之间的粘结力。采用FDM技术,使用丙烯腈-丁二烯-苯乙烯(ABS)、聚对苯二甲酸乙二醇酯共聚聚酯(PETG)和高抗冲聚苯乙烯(HIPS)打印CAD设计的实验测试块,参考测试块由传统光固化树脂制成(n = 11)。在GB处理前后,分析了所有托盘材料的表面形貌,并测量了从硅橡胶印模/粘结系统上剥离的测试块的最大强度。GB处理后,四个材料组的算术平均高度(Sa)和谷底储液指数(Svi)均下降(< 0.05)。四个材料组各自的剥离强度均因GB处理而显著降低(< 0.05),但在GB处理前后它们之间未发现统计学差异。在所有剥离试验中,粘结破坏均发生在粘结剂-印模材料界面。结果表明,ABS、HIPS和PETG与传统光固化树脂一样,能够为粘结剂提供足够的粘结力,并且GB处理可以降低FDM产生的粗糙度,并削弱粘结剂与硅橡胶印模之间的粘结。