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煅烧过程对通过蜂蜜辅助燃烧法制备的用于抗菌性能的CdO-ZnO纳米复合材料的影响。

Effect of the calcination process on CdO-ZnO nanocomposites by a honey-assisted combustion method for antimicrobial performance.

作者信息

Somasundaram Gopi, Rajan Jayaprakash, Paul Justin

机构信息

Department of Physics , Nanotechnology laboratory , Sri Ramakrishna Mission Vidyalaya College of Arts and Science , Coimbatore-641020 , India . Email:

出版信息

Toxicol Res (Camb). 2018 May 11;7(5):779-791. doi: 10.1039/c8tx00059j. eCollection 2018 Sep 1.

Abstract

This work reports on honey as a combustion agent of CdO : ZnO nanocomposites and the effects of further annealing (100 °C, 200 °C, 300 °C and 400 °C) on their structural, optical, morphological, elemental, electrical and antimicrobial properties are investigated. X-ray diffraction spectra confirm the cubic and hexagonal structure of CdO : ZnO nanocomposites at 400 °C. When the calcination temperature was increased, the crystallinity, absorbance, bandgap, luminescence intensity, morphological dispersion and mean particle size were also increased. HR-TEM imaging confirmed spherical particles with an average particle size of ∼49 nm. The electrical conductivity of the CdO : ZnO nanoparticles was investigated. The antimicrobial activity of CdO : ZnO nanocomposites was tested for various bacterial and fungal organisms using a zone inhibition method.

摘要

这项工作报道了蜂蜜作为CdO : ZnO纳米复合材料的燃烧剂,并研究了进一步退火(100°C、200°C、300°C和400°C)对其结构、光学、形态、元素、电学和抗菌性能的影响。X射线衍射光谱证实了CdO : ZnO纳米复合材料在400°C时的立方和六方结构。当煅烧温度升高时,结晶度、吸光度、带隙、发光强度、形态分散性和平均粒径也会增加。高分辨率透射电子显微镜成像证实了平均粒径约为49 nm的球形颗粒。研究了CdO : ZnO纳米颗粒的电导率。使用抑菌圈法测试了CdO : ZnO纳米复合材料对各种细菌和真菌的抗菌活性。

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