He Jun, Xu Jie-Kun, Pan Xue-Ge, Ye Xian-Sheng, Liang Ying-Ying, Yang Ge-Fan, Zhang Wei-Ku
Department of Pharmacy, China-Japan Friendship Hospital, Beijing 100029, China.
School of Life Sciences, Beijing University of Chinese Medicine, Beijing 100029, China.
Zhongguo Zhong Yao Za Zhi. 2018 Nov;43(21):4264-4266. doi: 10.19540/j.cnki.cjcmm.2018.0113.
To investigate the chemical compounds from the ripe fruit of Cornus officinalis, a new phenylpropanoid glycoside 1-O-(6'-O-p-hydroxybenzoyl-β-D-glucopyranosyl)-p-phenylpropanol, named cornuphenylpropanoid A (1), were separated and purified by D101 macroporous resin, silica gel and ODS column chromatography. Its structure was extensively determined on basis of ¹H-NMR, ¹³C-NMR, DEPT, HSQC, HMBC and HR-ESI-MS spectroscopic data.
为了研究山茱萸成熟果实中的化学成分，通过D101大孔树脂、硅胶和ODS柱色谱法分离并纯化了一种新的苯丙素苷1-O-(6'-O-对羟基苯甲酰基-β-D-吡喃葡萄糖基)-对苯丙醇，命名为山茱萸苯丙素A(1)。基于¹H-NMR、¹³C-NMR、DEPT、HSQC、HMBC和HR-ESI-MS光谱数据对其结构进行了广泛的测定。
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