López-Miranda J Luis, Esparza R, Rosas G, Pérez R, Estévez-González M
1Centro de Física Aplicada y Tecnología Avanzada, Universidad Nacional Autónoma de México, Boulevard Juriquilla 3001, 76230 Santiago de Querétaro, Querétaro Mexico.
2Instituto de Investigaciones Metalúrgicas, UMSNH, edificio U, ciudad universitaria, 58060 Morelia Michoacán, Mexico.
3 Biotech. 2019 Apr;9(4):135. doi: 10.1007/s13205-019-1666-z. Epub 2019 Mar 9.
In this work, we are proposing the green synthesis of gold nanoparticles (AuNPs) using aqueous extracts of and evaluating their antibacterial and catalytic properties. Characterization was performed by UV-Vis and FT-IR spectroscopies, X-ray diffraction, and transmission electron microscopy (TEM). Antibacterial activity of AuNPs was analyzed using and and catalytic activity was determined by the degradation of methylene blue and congo red. UV-Vis analysis showed an increase in AuNPs concentration by increasing the extract concentration, volume extract, and precursor salt concentration. The crystalline nature of AuNPs was corroborated by X-ray diffraction. TEM analysis showed nanoparticles with spherical morphology (mostly) and size between 40 and 60 nm. These results are novel because they showed a homogeneous morphology and a narrow size distribution which is difficult to obtain in green synthesis processes. Results of antibacterial activity showed inhibition zones of 11.3 mm and 10.6 mm for and , respectively, indicating the bactericidal capacity of the nanoparticles. The degradation periods for methylene blue and congo red were 5 and 11 min, respectively, which are very short compared with previous reports. These results are of great significance for catalytic applications. Therefore, extracts made possible AuNPs synthesis and the nanoparticles obtained can be used as catalytic and antibacterial materials for water remediation.
在本工作中,我们提出使用[植物名称]水提取物绿色合成金纳米粒子(AuNPs),并评估其抗菌和催化性能。通过紫外可见光谱和傅里叶变换红外光谱、X射线衍射以及透射电子显微镜(TEM)进行表征。使用[细菌名称1]和[细菌名称2]分析AuNPs的抗菌活性,并通过亚甲基蓝和刚果红的降解来测定催化活性。紫外可见分析表明,通过增加提取物浓度、提取物体积和前体盐浓度,AuNPs浓度增加。X射线衍射证实了AuNPs的晶体性质。TEM分析显示纳米粒子主要呈球形形态,尺寸在40至60纳米之间。这些结果是新颖的,因为它们显示出均匀的形态和窄的尺寸分布,这在绿色合成过程中很难获得。抗菌活性结果表明,对[细菌名称1]和[细菌名称2]的抑菌圈分别为11.3毫米和10.6毫米,表明纳米粒子的杀菌能力。亚甲基蓝和刚果红的降解时间分别为5分钟和11分钟,与先前的报道相比非常短。这些结果对催化应用具有重要意义。因此,[植物名称]提取物使得AuNPs的合成成为可能,所获得的纳米粒子可作为水修复的催化和抗菌材料。