Femi-Adepoju Abiola Grace, Dada Adewumi Oluwasogo, Otun Kabir Opeyemi, Adepoju Adeyinka Olufemi, Fatoba Ojo Paul
Department of Plant and Environmental Biology, Kwara State University, Malete, Kwara State, Nigeria.
Department of Physical Sciences, Nanotechnology Laboratory, Industrial Chemistry Programme, Landmark University, Nigeria.
Heliyon. 2019 Apr 23;5(4):e01543. doi: 10.1016/j.heliyon.2019.e01543. eCollection 2019 Apr.
Novel silver nanoparticles from Willd.) C. Presl. was synthesized. A combination of spectroscopic and microscopic techniques were utilized to characterize the newly synthesized Silver Nanoparticles (GPAgNPs) vis-à-vis UV-Vis Spectroscopy, Fourier Transform Infra-Red (FTIR) Spectroscopy, Scanning Electron Microscopy (SEM), Transmission Electron Microscopy (TEM), Energy Dispersive X-ray Spectroscopy (EDX) and X-Ray Diffraction (XRD) Analyses. Significant absorption was observed at 460 nm resulting from the surface Plasmon resonance (SPR). A rapid rate of synthesis was observed and the best surface plasmon resonance was obtained at 105 minutes contact time. SEM and TEM showed an spherical shape of GPAgNPs with an average size of 7.51 nm. The XRD result revealed a crystalline and polydispersed GPAgNPs. GPAgNPs were effective against four antibiotic resistant pathogens and they exhibited excellent antimicrobial activity against , and GPAgNPs favorably competed with standard antibiotics. This therefore enlisted GPAgNPs as potential antimicrobial and therapeutic agents against multidrug resistant micro-organisms (MDRM).
合成了来自Willd.) C. Presl.的新型银纳米颗粒。利用光谱和显微镜技术相结合的方法,通过紫外可见光谱、傅里叶变换红外光谱、扫描电子显微镜、透射电子显微镜、能量色散X射线光谱和X射线衍射分析等手段对新合成的银纳米颗粒(GPAgNPs)进行表征。由于表面等离子体共振(SPR),在460nm处观察到显著吸收。观察到快速的合成速率,在接触时间为105分钟时获得了最佳的表面等离子体共振。扫描电子显微镜和透射电子显微镜显示GPAgNPs呈球形,平均尺寸为7.51nm。X射线衍射结果表明GPAgNPs是结晶的且多分散。GPAgNPs对四种耐抗生素病原体有效,并且它们对、和表现出优异的抗菌活性。GPAgNPs与标准抗生素具有良好的竞争能力。因此,这使GPAgNPs成为对抗多重耐药微生物(MDRM)的潜在抗菌和治疗剂。