Kumar Naresh, Zafar Muhammad S, Dahri Waheed M, Khan Muhammad A, Khurshid Zohaib, Najeeb Shariq
Department of Science of Dental Materials, Dow International Dental College, Dow University of Health Sciences, Karachi, Pakistan.
Department of Restorative Dentistry, College of Dentistry, Taibah University, Almadinah Almunawwarah, KSA.
J Taibah Univ Med Sci. 2018 Jun 6;13(4):319-326. doi: 10.1016/j.jtumed.2018.04.012. eCollection 2018 Aug.
This study aimed to determine the biaxial flexural strength (BFS) of resin composite materials at distinct deformation rates.
Two micro-hybrid [Filtek Z100™ Restorative (Z100), Filtek™ Z250 (Z250)] and two nano-filled [Filtek™ Supreme XT Body (FSB), Filtek™ Supreme Translucent (FST)] composite resins were selected. Disc-shaped (12 × 1 mm) specimens were fabricated using nylon split moulds. Bar-shaped specimens (25 × 2 × 2 mm) were fabricated from each material to determine the flexural modulus. The specimens were tested for BFS and flexural modulus under dry and wet conditions after 1, 13, and 52 weeks.
The highest BFS was recorded for Z250 (162 ± 19 MPa), followed by FST (154 ± 16 MPa), Z100 (150 ± 18 MPa), and FSB (136 ± 18 MPa). The materials exhibited a clear trend of increase in BFS with deformation rate. Following immersion for 1 week, the BFS was 126 ± 18 MPa for Z100, and 124 ± 17 MPa for Z250, which were higher than those of FSB (99 ± 16 MPa) and FST (115 ± 19 MPa) under comparable conditions. There was a remarkable reduction in the flexural moduli of the specimens immersed for 1 week compared to those of the dry specimens: Z100 (from 18.3 ± 1.2 GPa for dry specimen to 15.7 ± 0.8 GPa after immersion for 1 week), Z250 (from 16.7 ± 0.8 GPa to 13.3 ± 1.4 GPa), FSB (from 13.7 ± 0.6 GPa to 11.0 ± 2.1 GPa) and FST (from 12.7 ± 2.3 GPa to 10.4 ± 1.0 GPa).
This study concludes that the BFS and flexural moduli of resin-based dental restoratives decline when they are immersed in an aqueous medium until saturation with water. However, after equilibrium is established, the immersion medium does not affect the restorative materials further. Variations in deformation rate did not have a significant effect on the BFS of resin-based dental restoratives.
本研究旨在测定树脂复合材料在不同变形速率下的双轴弯曲强度(BFS)。
选择两种微混合树脂[Filtek Z100™ 修复材料(Z100)、Filtek™ Z250(Z250)]和两种纳米填充树脂[Filtek™ Supreme XT Body(FSB)、Filtek™ Supreme Translucent(FST)]复合树脂。使用尼龙分体模具制作圆盘形(12×1mm)试件。从每种材料制作条形试件(25×2×2mm)以测定弯曲模量。在1周、13周和52周后,对试件在干燥和潮湿条件下进行BFS和弯曲模量测试。
Z250的BFS最高(162±19MPa),其次是FST(154±16MPa)、Z100(150±18MPa)和FSB(136±18MPa)。材料的BFS随变形速率呈现明显的增加趋势。浸泡1周后,Z100的BFS为126±18MPa,Z250为124±17MPa,在可比条件下高于FSB(99±16MPa)和FST(115±19MPa)。与干燥试件相比,浸泡1周的试件弯曲模量显著降低:Z100(从干燥试件的18.3±1.2GPa降至浸泡1周后的15.7±0.8GPa)、Z250(从16.7±0.8GPa降至13.3±1.4GPa)、FSB(从13.7±0.6GPa降至11.0±2.1GPa)和FST(从12.7±2.3GPa降至10.4±1.0GPa)。
本研究得出结论,树脂基牙科修复材料浸泡在水性介质中直至水饱和时,其BFS和弯曲模量会下降。然而,在达到平衡后,浸泡介质不会进一步影响修复材料。变形速率的变化对树脂基牙科修复材料的BFS没有显著影响。