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绿色合成的植物化学物质（姜和大蒜）还原的氧化镍纳米颗粒证实了杀菌和催化潜力。

Green Synthesized Phytochemically (Zingiber officinale and Allium sativum) Reduced Nickel Oxide Nanoparticles Confirmed Bactericidal and Catalytic Potential.

作者信息

Haider Ali, Ijaz Muhammad, Ali Sidra, Haider Junaid, Imran Muhammad, Majeed Hamid, Shahzadi Iram, Ali Muhammad Muddassir, Khan Jawaria Ali, Ikram Muhammad

机构信息

Department of Clinical Medicine and Surgery, University of Veterinary and Animal Sciences, Lahore, Punjab, 54000, Pakistan.

Department of Gynaecology& Obstetric (Unit -III), Jinnah Hospital, Lahore, Punjab, 54000, Pakistan.

出版信息

Nanoscale Res Lett. 2020 Mar 2;15(1):50. doi: 10.1186/s11671-020-3283-5.

DOI:10.1186/s11671-020-3283-5
PMID:32124107
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC7052104/
Abstract

Phyto-synthesized nanoparticles (NPs) having reduced chemical toxicity have been focused globally and become essential component of nanotechnology recently. We prepared green phytochemically (ginger and garlic) reduced NiO-NPs to replace synthetic bactericidal and catalytic agent in textile industry. NPs were characterized using ultra-violet visible spectroscopy (UV-Vis), X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), Fourier-transform infrared spectroscopy (FTIR), energy-dispersive X-ray spectroscopy (EDS), scanning electron microscopy (SEM), and transmission electron microscopy (TEM). The synthesis of NPs was confirmed by XRD and UV-Vis having strong absorption at 350 nm with size ranged between 16-52 nm for ginger and 11-59 nm for garlic. Scanning and transmission electron microscopy confirmed pleomorphism with cubic- and more spherical-shaped NPs. Moreover, exact quantities of garlic and ginger extracts (1:3.6 ml) incorporated to synthesize NiO-NPs have been successfully confirmed by FTIR. Phytochemically reduced NPs by garlic presented enhanced bactericidal activity against multiple drug-resistant Staphylococcus aureus at increasing concentrations (0.5, 1.0 mg/50 μl) and also degraded methylene blue (MB) dye efficiently. Conclusively, green synthesized NiO-NPs are impending activists to resolve drug resistance as well as environment friendly catalytic agent that may be opted at industrial scale.

摘要

具有降低化学毒性的植物合成纳米颗粒（NPs）已在全球范围内受到关注，并成为近年来纳米技术的重要组成部分。我们通过植物化学方法（使用生姜和大蒜）制备了还原型NiO-NPs，以替代纺织工业中的合成杀菌剂和催化剂。使用紫外可见光谱（UV-Vis）、X射线衍射（XRD）、X射线光电子能谱（XPS）、傅里叶变换红外光谱（FTIR）、能量色散X射线光谱（EDS）、扫描电子显微镜（SEM）和透射电子显微镜（TEM）对纳米颗粒进行了表征。XRD和UV-Vis证实了纳米颗粒的合成，在350nm处有强烈吸收，生姜合成的纳米颗粒尺寸在16-52nm之间，大蒜合成的纳米颗粒尺寸在11-59nm之间。扫描电子显微镜和透射电子显微镜证实了纳米颗粒的多形性，呈现立方体形和更多球形。此外，FTIR成功证实了用于合成NiO-NPs的大蒜和生姜提取物的确切用量（1:3.6ml）。大蒜植物化学还原的纳米颗粒在浓度增加时（0.5、1.0mg/50μl）对多重耐药金黄色葡萄球菌表现出增强的杀菌活性，并且还能有效降解亚甲基蓝（MB）染料。总之，绿色合成的NiO-NPs是解决耐药性问题的潜在活性剂，也是一种可在工业规模上选用的环境友好型催化剂。

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