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光固化树脂水门汀物理和力学性能的体外评价:一项对比研究。

In Vitro Evaluation of Physical and Mechanical Properties of Light-Curing Resin Cement: A Comparative Study.

作者信息

Espíndola-Castro Luís Felipe, Brito Oscar Felipe Fonseca de, Araújo Larissa Gabrielle Assis, Santos Izabella Luiza Aragão, Monteiro Gabriela Queiroz De Melo

机构信息

Dental School, Faculdade de Odontologia de Pernambuco, Universidade de Pernambuco (FOP/UPE), Camaragibe, Brazil.

出版信息

Eur J Dent. 2020 Feb;14(1):152-156. doi: 10.1055/s-0040-1705075. Epub 2020 Mar 13.

Abstract

OBJECTIVE

The aim of study was to evaluate the surface hardness, sorption, solubility, and color stability of three light-cured resin cements, namely RelyX Veneer (RLX), Variolink Veneer (VLK), and All Cem Veneer (ACV).

MATERIALS AND METHODS

Cylindrical samples (15 × 1 mm) were made for each group using a metallic mold ( = 10). Vickers microhardness test was performed, and average hardness was calculated from three indentations (300 gf/15s) per sample. The sorption and solubility of the materials were evaluated according to ISO 4049:2009 based on three samples weighing: initial ( ), after immersion in distilled water for 7 days ( ), and final (after removal of all moisture [ ]). The color change was observed using a digital spectrophotometer, at three different time points, baseline, 1 day, and 1 week of immersion in coffee and distilled water (control).

STATISTICAL ANALYSIS

Shapiro-Wilk test was used to analyze the normality of the data, and groups were compared using Kruskal-Wallis and Mann-Whitney tests. A significance level of 5% was used.

RESULTS

RLX showed the highest microhardness mean values (36.96 VHN), but higher sorption (23.2 µg/mm) and solubility (2.40 µg/mm), with statistically significant differences with the other groups. For color stability, higher ∆E was observed for the samples immersed in coffee ( = 0.009). The VLK resin cement presented statistically significant differences from the other groups, with higher color changes in coffee at 1 day (15.14) and after 1 week (23.65).

CONCLUSION

RLX resin cement showed better hardness results. All materials tested performed satisfactorily for sorption and solubility according to ISO 4049:2009. All materials showed high-staining values after 1 week of immersion in coffee.

摘要

目的

本研究旨在评估三种光固化树脂水门汀,即丽素美贴面树脂(RLX)、Variolink贴面树脂(VLK)和全瓷贴面树脂水门汀(ACV)的表面硬度、吸附性、溶解性和颜色稳定性。

材料与方法

使用金属模具为每组制作圆柱形样本(15×1毫米)(每组n = 10)。进行维氏显微硬度测试,并从每个样本的三次压痕(300克力/15秒)计算平均硬度。根据ISO 4049:2009,基于三个样本重量评估材料的吸附性和溶解性:初始重量(W1)、在蒸馏水中浸泡7天后的重量(W2)和最终重量(去除所有水分后的重量[W3])。使用数字分光光度计在三个不同时间点观察颜色变化,即基线、浸泡在咖啡和蒸馏水中1天以及1周(对照)。

统计分析

使用夏皮罗-威尔克检验分析数据的正态性,并使用克鲁斯卡尔-沃利斯检验和曼-惠特尼检验比较各组。显著性水平设定为5%。

结果

RLX显示出最高的显微硬度平均值(36.96维氏硬度),但吸附性(23.2微克/毫米)和溶解性(2.40微克/毫米)较高,与其他组存在统计学显著差异。对于颜色稳定性,浸泡在咖啡中的样本观察到更高的∆E值(P = 0.009)。VLK树脂水门汀与其他组存在统计学显著差异,在咖啡中1天时颜色变化较高(15.14),1周后颜色变化较高(23.65)。

结论

RLX树脂水门汀显示出更好的硬度结果。根据ISO 4049:2009,所有测试材料在吸附性和溶解性方面表现令人满意。所有材料在浸泡在咖啡中1周后均显示出高染色值。

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本文引用的文献

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Color Stability of Resin Cements Exposed to Aging.树脂水门汀老化后的颜色稳定性。
Oper Dent. 2019 Nov/Dec;44(6):609-614. doi: 10.2341/18-064-L. Epub 2019 Jan 31.

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