Department of Physical and Chemical Analysis, Fujian Provincial Key Laboratory of Zoonosis Research, Fujian Center for Disease Control and Prevention , Fuzhou, China.
Food Addit Contam Part B Surveill. 2020 Sep;13(3):177-184. doi: 10.1080/19393210.2020.1751309. Epub 2020 Apr 20.
Thirty-nine kinds of antibiotics (11 quinolones, 10 tetracyclines, and 18 sulphonamides) residues were screened in 146 samples including chicken, chicken giblets, and eggs in Fujian by ultra-performance liquid chromatography-tandem mass spectrometry (LC-MS/MS) and analysed the contamination status of antibiotic residues.seventeen kinds of antibiotics were detected, with an overall detection rate of 47.3% and the exceeding rate was 11.6%. Antibiotics were found in 46.7% chicken, 72.2% chicken giblets, and 30% eggs. In 11.1% of chicken giblets and 26% of eggs, the detected concentration exceeded the maximum residue level (MRLs). The total detection rate of tetracycline antibiotics was higher than that of quinolones (33.6% vs. 24.7%) and the sulphonamides (33.6% vs. 4.8%). The exceeding rates of tetracyclines, quinolones, and sulphonamides were 2.7%, 10.3%, and 1.4%, respectively. We suggested that the abuse of antibiotics in poultry foods still exists, and more attention should be paid to the antibiotic residues in poultry eggs.
采用超高效液相色谱-串联质谱法(LC-MS/MS)对福建省 146 份鸡肉、鸡杂和鸡蛋样品进行了 11 种喹诺酮类、10 种四环素类和 18 种磺胺类共 39 种抗生素残留筛查,并分析了抗生素残留污染状况。共检出 17 种抗生素,总体检出率为 47.3%,超标率为 11.6%。抗生素在鸡肉中的检出率为 46.7%,鸡杂中的检出率为 72.2%,鸡蛋中的检出率为 30%。在 11.1%的鸡杂和 26%的鸡蛋中,检测到的浓度超过了最大残留限量(MRLs)。四环素类抗生素的总检出率高于喹诺酮类(33.6%比 24.7%)和磺胺类(33.6%比 4.8%)。四环素类、喹诺酮类和磺胺类的超标率分别为 2.7%、10.3%和 1.4%。结果表明,禽肉食品中抗生素的滥用仍然存在,应更加关注禽蛋中的抗生素残留。