Am J Orthod. 1977 Jun;71(6):637-50. doi: 10.1016/0002-9416(77)90280-9.
After etching for one minute with 35 per cent phosphoric acid, thirty-eight permanent teeth were furnished with plastic brackets. An additional twelve teeth were used as references and were etched but were not furnished with brackets. Four teeth served as untreated controls. Eight brackets had fallen off one week later. The remaining brackets were removed with various instruments. All the teeth were extracted and examined by scanning electron microscopy (SEM). On all of the teeth originally furnished with brackets, residual acrylic was found on the tooth surface. The SEM examination was supplemented with energy-dispersive x-ray analysis (ED) which confirmed that the observed residues differed in their chemical composition from the dental substance.
用35%的磷酸蚀刻一分钟后,为38颗恒牙安装了塑料托槽。另外12颗牙齿用作对照,进行了蚀刻但未安装托槽。4颗牙齿作为未处理的对照。一周后有8个托槽脱落。其余托槽用各种器械取下。所有牙齿均拔除并通过扫描电子显微镜(SEM)检查。在所有最初安装托槽的牙齿表面均发现有残留的丙烯酸树脂。扫描电子显微镜检查辅以能量色散X射线分析(ED),证实观察到的残留物的化学成分与牙质不同。