School of Food Science and Technology, Kyungpook National University, Daegu 41566, South Korea.
School of Food Science and Technology, Kyungpook National University, Daegu 41566, South Korea.
Food Chem. 2021 Feb 15;338:128150. doi: 10.1016/j.foodchem.2020.128150. Epub 2020 Sep 22.
This study aimed to develop efficient adsorption and desorption processes to purify phenolic compounds from Ecklonia cava. We compared the adsorption and desorption properties of five resins. HP2MG showed the highest adsorption and desorption capacities and adsorption rate; hence, it was selected for phenolic compound purification. Adsorption isotherm parameters indicated favorable adsorption between HP2MG and phenolic compounds. Thermodynamic parameters showed that the absorption process physically proceeded. In the dynamic adsorption process, adsorption property was assessed based on bed length (4-10 cm) and flow rate (1.64-3.27 mL/min). The breakthrough point increased with increased bed length and decreased adsorption flow rate. However, the high desorption flow rate shortened the processing time. The phenolic contents, anti-glycation activity and antioxidant activity of the extract were measured before and after purification. The dieckol and phlorofucofuroeckol-A increased three times after purification. The purified extract showed higher anti-glycation and antioxidant activities than the extract.
本研究旨在开发有效的吸附和解吸工艺,从裙带菜中纯化酚类化合物。我们比较了五种树脂的吸附和解吸性能。HP2MG 表现出最高的吸附和解吸容量和吸附速率,因此被选择用于酚类化合物的纯化。吸附等温线参数表明 HP2MG 与酚类化合物之间存在有利的吸附作用。热力学参数表明,吸收过程是物理进行的。在动态吸附过程中,基于床层长度(4-10cm)和流速(1.64-3.27mL/min)评估吸附性能。随着床层长度的增加和吸附流速的降低,穿透点增加。然而,高的解吸流速缩短了处理时间。测定了纯化前后提取物的酚类含量、抗糖化活性和抗氧化活性。纯化后,二酮和 phlorofucofuroeckol-A 增加了三倍。纯化后的提取物显示出比提取物更高的抗糖化和抗氧化活性。