Fang Zhiyong, Guo Yanhui, Fu Bin, Wei Liqun, Chen Jun, Pang Linghuan, Wang Zemin
School of Materials Science and Engineering, Shanghai Institute of Technology, Shanghai 201418, China.
Materials (Basel). 2020 Oct 22;13(21):4696. doi: 10.3390/ma13214696.
In the present work, the microstructure and texture of non-oriented 3.3% Si steel processed by asymmetric rolling (ASR) and subsequent annealing at different temperatures were compared with those obtained when using traditional symmetric rolling (SR). This work aims to reveal the effect of shear bands introduced by the ASR on the microstructure and texture evolution. The ASR sample reaches a recrystallization fraction of 62% at an annealing temperature of 650 °C, which is 32% higher than that of the SR sample annealed at the same temperature. This can be attributed to the abundant shear bands introduced by the ASR, which serve as the heterogeneous nucleation sites for the recrystallized grains. When increasing the annealing temperature to 750 °C, complete recrystallization could be observed in both asymmetric- and symmetric-rolled samples. When using an annealing temperature of 650 °C, the γ-oriented grains were dominant in the surface layer, while strong Goss-oriented grains could be observed in the center in the ASR sample. This is due to the fragmented small subgrains with different orientations in the surface layer inhibiting the nucleation of Goss- and cube-oriented grains during the annealing. In contrast, numerous Goss- and cube-oriented grains were formed in the surface layer after complete recrystallization when the ASR sample was annealed at a temperature of 750 °C. This may be related to the higher thermal energy, which benefits the nucleation of the Goss- and cube-oriented grains. In addition, ASR significantly increased the strength of η-fiber after complete recrystallization when compared with SR. This work might be helpful to design the rolling and the subsequent annealing processes.
在本研究中,将非取向3.3%硅钢经异步轧制(ASR)及随后在不同温度下退火后的微观结构和织构,与采用传统同步轧制(SR)时获得的微观结构和织构进行了比较。本研究旨在揭示异步轧制引入的剪切带对微观结构和织构演变的影响。异步轧制样品在650℃退火温度下达到62%的再结晶分数,比在相同温度下退火的同步轧制样品高32%。这可归因于异步轧制引入的大量剪切带,其作为再结晶晶粒的异质形核位点。当退火温度升至750℃时,在异步和同步轧制样品中均观察到完全再结晶。当采用650℃退火温度时,γ取向晶粒在表层占主导,而在异步轧制样品的中心可观察到较强的高斯取向晶粒。这是由于表层中具有不同取向的破碎小亚晶粒在退火过程中抑制了高斯取向和立方取向晶粒的形核。相比之下,当异步轧制样品在750℃温度下退火完全再结晶后,表层形成了大量高斯取向和立方取向晶粒。这可能与较高的热能有关,这有利于高斯取向和立方取向晶粒的形核。此外,与同步轧制相比,异步轧制在完全再结晶后显著提高了η纤维的强度。本研究可能有助于设计轧制及随后的退火工艺。