Yang Wendi, Zhang Chengzhi, Zhang Nan, Zhang Chucan, Gao Weilin, He Jilin
School of Material Science and Engineering, Zhengzhou University, Zhengzhou 450001, China.
Zhongyuan Critical Metals Laboratory, Zhengzhou 450001, China.
Materials (Basel). 2024 Jun 3;17(11):2696. doi: 10.3390/ma17112696.
The microstructure and texture evolution of Cu-Ni-P alloy after cold rolling and annealing at 500 °C was studied by electron backscattering diffraction (EBSD). The equiaxed grain is elongated and the dislocation density increases gradually after cold rolling. The grain boundaries become blurred and the structure becomes banded when the reduction in cold rolling reaches 95%. A typical rolling texture is formed with the increase in deformation amount in cold rolling. The deformation structure gradually disappeared and recrystallized new grains were formed after annealing at 500 °C. The recrystallization nucleation mechanism of Cu-Ni-P alloy at 60% reduction is mainly a bow nucleation mechanism. A shear band begins to form after annealing at 80% reduction. The shear band becomes the preferred nucleation location with the increase in reduction. Most adjacent recrystallized grains growing in the shear band have a twin relationship.
采用电子背散射衍射(EBSD)技术研究了Cu-Ni-P合金冷轧及500℃退火后的微观组织与织构演变。冷轧后等轴晶粒被拉长,位错密度逐渐增加。当冷轧压下率达到95%时,晶界变得模糊,组织呈带状。随着冷轧变形量的增加,形成了典型的轧制织构。500℃退火后,变形组织逐渐消失并形成再结晶新晶粒。60%压下率时Cu-Ni-P合金的再结晶形核机制主要为弓出形核机制。80%压下率退火后开始形成剪切带。随着压下率的增加,剪切带成为优先形核位置。在剪切带中生长的大多数相邻再结晶晶粒具有孪晶关系。