Dufresne Eric M, Narayanan Suresh, Reininger Ruben, Sandy Alec R, Lurio Larry
Advanced Photon Source, Argonne National Laboratory, Argonne, IL 60439, USA.
Department of Physics, Northern Illinois University, DeKalb, IL, USA.
J Synchrotron Radiat. 2020 Nov 1;27(Pt 6):1528-1538. doi: 10.1107/S1600577520012163. Epub 2020 Oct 20.
This paper illustrates the use of spatial filtering with a horizontal slit near the source to enlarge the horizontal coherence in an experimental station and produce a diffraction-limited round focus at an insertion device beamline for X-ray photon correlation spectroscopy experiments. Simple expressions are provided to guide the optical layout, and wave propagation simulations confirm their applicability. The two-dimensional focusing performance of Be compound refractive lenses to produce a round diffraction-limited focus at 11 keV capable of generating a high-contrast speckle pattern of an aerogel sample is demonstrated. The coherent scattering patterns have comparable speckle sizes in both horizontal and vertical directions. The focal spot sizes are consistent with hybrid ray-tracing calculations. Producing a two-dimensional focus on the sample can be helpful to resolve speckle patterns with modern pixel array detectors with high visibility. This scheme has now been in use since 2019 for the 8-ID beamline at the Advanced Photon Source, sharing the undulator beam with two separate beamlines, 8-ID-E and 8-ID-I at 7.35 keV, with increased partially coherent flux, reduced horizontal spot sizes on samples, and good speckle contrast.
本文阐述了在光源附近使用带有水平狭缝的空间滤波,以扩大实验站的水平相干性,并在用于X射线光子相关光谱实验的插入式设备光束线上产生衍射极限圆形焦点。提供了简单的表达式来指导光学布局,并且波传播模拟证实了它们的适用性。展示了铍复合折射透镜在11 keV时产生圆形衍射极限焦点的二维聚焦性能,该焦点能够生成气凝胶样品的高对比度散斑图案。相干散射图案在水平和垂直方向上具有相当的散斑尺寸。焦斑尺寸与混合光线追迹计算结果一致。在样品上产生二维焦点有助于使用具有高可见度的现代像素阵列探测器解析散斑图案。该方案自2019年起已在先进光子源的8-ID光束线中使用,与7.35 keV的两条独立光束线8-ID-E和8-ID-I共享波荡器光束,具有增加的部分相干通量、减小的样品上水平光斑尺寸以及良好的散斑对比度。