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元素混合 Ti-Mo 和 Ti-Mo-Zr 合金中β相稳定性的影响。

Influence of β-phase stability in elemental blended Ti-Mo and Ti-Mo-Zr alloys.

机构信息

Department of Production and Industrial Engineering, Polytechnic University of Valencia, Valencia, 46022, Spain.

Department of Mechanical Engineering, Sandip Institute of Technology and Research Centre, Nashik, 422213, India.

出版信息

Micron. 2021 Mar;142:102992. doi: 10.1016/j.micron.2020.102992. Epub 2020 Dec 3.

Abstract

This paper investigated the improvement of mechanical properties for one of the most used biomaterials, titanium-based alloy. To improve its mechanical properties, molybdenum was chosen to be added to Ti and Ti-Zr alloys through a mechanical blending process. After homogenization of Ti (12, 15) Mo and Ti (12, 15) Mo-6 Zr, the compaction pressure and sintering temperature were varied to create pellets. Characterization has been done using scanning electron microscopy (SEM), X-ray diffraction (XRD), Vickers's hardness, Archimedes test and ultrasonic method, and 3-point bending test. Micrograph of each pellet revealed the influence of Mo content that plays a prominent role in the variation of microstructure in the alloys Ti-Mo and Ti-Zr-Mo. The porosity and density were also influenced by changing the β-phase. EBSD analysis shows the increase in β-phase with the addition of Zr. The overall results indicated that the percentage of β-phase greatly affects the mechanical properties for the specimens.

摘要

本文研究了一种最常用的生物材料——钛基合金的力学性能的提高。为了改善其力学性能,通过机械混合工艺选择钼来添加到 Ti 和 Ti-Zr 合金中。在 Ti(12,15)Mo 和 Ti(12,15)Mo-6Zr 均匀化后,改变压实压力和烧结温度来制备压坯。使用扫描电子显微镜(SEM)、X 射线衍射(XRD)、维氏硬度、阿基米德测试和超声波方法以及三点弯曲测试对其进行了表征。每个压坯的微观照片显示了 Mo 含量的影响,Mo 含量在 Ti-Mo 和 Ti-Zr-Mo 合金的微观结构变化中起着重要作用。孔隙率和密度也受到β相变化的影响。EBSD 分析表明,Zr 的添加会增加β相。总体结果表明,β相的百分比极大地影响了试样的力学性能。

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