Department of Production and Industrial Engineering, Polytechnic University of Valencia, Valencia, 46022, Spain.
Department of Mechanical Engineering, Sandip Institute of Technology and Research Centre, Nashik, 422213, India.
Micron. 2021 Mar;142:102992. doi: 10.1016/j.micron.2020.102992. Epub 2020 Dec 3.
This paper investigated the improvement of mechanical properties for one of the most used biomaterials, titanium-based alloy. To improve its mechanical properties, molybdenum was chosen to be added to Ti and Ti-Zr alloys through a mechanical blending process. After homogenization of Ti (12, 15) Mo and Ti (12, 15) Mo-6 Zr, the compaction pressure and sintering temperature were varied to create pellets. Characterization has been done using scanning electron microscopy (SEM), X-ray diffraction (XRD), Vickers's hardness, Archimedes test and ultrasonic method, and 3-point bending test. Micrograph of each pellet revealed the influence of Mo content that plays a prominent role in the variation of microstructure in the alloys Ti-Mo and Ti-Zr-Mo. The porosity and density were also influenced by changing the β-phase. EBSD analysis shows the increase in β-phase with the addition of Zr. The overall results indicated that the percentage of β-phase greatly affects the mechanical properties for the specimens.
本文研究了一种最常用的生物材料——钛基合金的力学性能的提高。为了改善其力学性能,通过机械混合工艺选择钼来添加到 Ti 和 Ti-Zr 合金中。在 Ti(12,15)Mo 和 Ti(12,15)Mo-6Zr 均匀化后,改变压实压力和烧结温度来制备压坯。使用扫描电子显微镜(SEM)、X 射线衍射(XRD)、维氏硬度、阿基米德测试和超声波方法以及三点弯曲测试对其进行了表征。每个压坯的微观照片显示了 Mo 含量的影响,Mo 含量在 Ti-Mo 和 Ti-Zr-Mo 合金的微观结构变化中起着重要作用。孔隙率和密度也受到β相变化的影响。EBSD 分析表明,Zr 的添加会增加β相。总体结果表明,β相的百分比极大地影响了试样的力学性能。