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气相色谱样品进样方法。

Sample Introduction Method in Gas Chromatography.

机构信息

Laboratory of Veterinary Public Health-1, School of Veterinary Medicine, Azabu University, 1-17-71 Fuchinobe Chuo, Sagamihara, Kanagawa, 252-5201, Japan.

Faculty of Pharmaceutical Sciences, Nagasaki International University, 2825-7 Huis Ten Bosch-cho Sasebo, Nagasaki, 859-3298, Japan.

出版信息

Anal Sci. 2021 Jan 10;37(1):159-165. doi: 10.2116/analsci.20SAR19. Epub 2020 Dec 18.

DOI:10.2116/analsci.20SAR19
PMID:33342926
Abstract

In this review, we summarize the methods of sample introduction into a gas chromatograph. For volatile organic compounds, headspace measurements and purge-trap methods have been used traditionally. Recently, the trapped headspace method has been used in water quality testing. In addition, various solid-state adsorption methods have been developed, including a method in which the adsorbent is placed inside a needle, while new adsorbents and their applications have also been introduced.

摘要

在这篇综述中,我们总结了将样品引入气相色谱仪的方法。对于挥发性有机化合物,传统上使用顶空测量和吹扫捕集方法。最近,捕集顶空法已用于水质测试。此外,还开发了各种固态吸附方法,包括将吸附剂置于针内的方法,同时还介绍了新的吸附剂及其应用。

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Characterization of the Aroma-Active Compounds in Commercial Fragrant Rapeseed Oils via Monolithic Material Sorptive Extraction.采用整体材料吸附萃取法对商品香油菜籽油中香气活性化合物的特征描述。
J Agric Food Chem. 2019 Oct 16;67(41):11454-11463. doi: 10.1021/acs.jafc.9b05691. Epub 2019 Oct 2.
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Profiling Single Cancer Cells with Volatolomics Approach.
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Volatile anticancer drug determination by thermal desorption technique with polydimethylsiloxane-coated macroporous silica adsorbent in gas chromatography-mass spectrometry.采用聚二甲基硅氧烷涂敷的大孔硅胶吸附剂的热解吸技术与气相色谱-质谱联用测定挥发性抗癌药物。
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Sampling bag-based emission chamber for measuring volatile organic compounds from household materials using solid-phase extraction-type collection device.基于采样袋的排放室,用于使用固相萃取型收集装置测量家用材料中的挥发性有机化合物。
Anal Sci. 2023 Oct;39(10):1615-1621. doi: 10.1007/s44211-023-00375-9. Epub 2023 May 30.
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Gas chromatographic determination of volatile compounds.气相色谱法测定挥发性化合物。
Anal Sci. 2022 May;38(5):737-738. doi: 10.1007/s44211-022-00108-4.
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Thermal Extraction of Polycyclic Aromatic Hydrocarbons from Atmospheric 2.5 μm Particulate Matter Collected on a Filter Paper Using a High-Temperature Headspace Method.利用高温顶空法从滤纸收集的大气 2.5μm 颗粒物中提取多环芳烃。
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