Serralta Eduardo, Klingner Nico, De Castro Olivier, Mousley Michael, Eswara Santhana, Duarte Pinto Serge, Wirtz Tom, Hlawacek Gregor
Institute of Ion Beam Physics and Materials Research, Helmholtz-Zentrum Dresden-Rossendorf, Bautzner Landstr. 400, 01328 Dresden, Germany.
Technische Universität Dresden, Dresden 01069, Germany.
Beilstein J Nanotechnol. 2020 Dec 11;11:1854-1864. doi: 10.3762/bjnano.11.167. eCollection 2020.
A detection system based on a microchannel plate with a delay line readout structure has been developed to perform scanning transmission ion microscopy (STIM) in the helium ion microscope (HIM). This system is an improvement over other existing approaches since it combines the information of the scanning beam position on the sample with the position (scattering angle) and time of the transmission events. Various imaging modes, such as bright field and dark field or the direct image of the transmitted signal, can be created by post-processing the collected STIM data. Furthermore, the detector has high spatial and temporal resolution, is sensitive to both ions and neutral particles over a wide energy range, and shows robustness against ion beam-induced damage. A special in-vacuum movable support gives the possibility of moving the detector vertically, placing the detector closer to the sample for the detection of high-angle scattering events, or moving it down to increase the angular resolution and distance for time-of-flight measurements. With this new system, we show composition-dependent contrast for amorphous materials and the contrast difference between small-angle and high-angle scattering signals. We also detect channeling-related contrast on polycrystalline silicon, thallium chloride nanocrystals, and single-crystalline silicon by comparing the signal transmitted at different directions for the same data set.
基于带有延迟线读出结构的微通道板开发了一种检测系统,用于在氦离子显微镜(HIM)中进行扫描透射离子显微镜(STIM)。该系统是对其他现有方法的改进,因为它将样品上扫描束位置的信息与透射事件的位置(散射角)和时间相结合。通过对收集到的STIM数据进行后处理,可以创建各种成像模式,如明场和暗场或透射信号的直接图像。此外,该探测器具有高空间和时间分辨率,在很宽的能量范围内对离子和中性粒子都敏感,并且对离子束诱导的损伤具有鲁棒性。一种特殊的真空可移动支架使得能够垂直移动探测器,将探测器放置得更靠近样品以检测大角度散射事件,或者将其向下移动以提高角分辨率和飞行时间测量的距离。使用这个新系统,我们展示了非晶材料的成分依赖性对比度以及小角度和大角度散射信号之间的对比度差异。我们还通过比较同一数据集在不同方向上传输的信号,检测了多晶硅、氯化铊纳米晶体和单晶硅上与沟道效应相关的对比度。