Abe Yoshifumi, Kurose Takashi, Santos Marcelo V A, Kanaya Yota, Ishigami Akira, Tanaka Shigeo, Ito Hiroshi
Department of Organic Materials Science, Graduate School of Organic Materials Science, Yamagata University, 4-3-16 Jonan, Yonezawa, Yamagata 992-8510, Japan.
Research Center for GREEN Materials & Advanced Processing, Yamagata University, 4-3-16 Jonan, Yonezawa, Yamagata 992-8510, Japan.
Materials (Basel). 2021 Jan 6;14(2):243. doi: 10.3390/ma14020243.
17-4PH stainless steel specimens were fabricated by fused deposition of metals (FDMet) technology, which combines 17-4PH particles with an organic binder. FDMet promises a low-cost additive manufacturing process. The present research aims to clarify the influence of layer directions in the 3D printing process on the mechanical and shrinkage properties of as-sintered and as-aged specimens. All specimens (the as-sintered and as-aged specimens printed in three layer directions) exhibited high relative density (97.5-98%). The highest ultimate strengths (880 and 1140 MPa in the as-sintered and as-aged specimens, respectively) were obtained when the layer direction was perpendicular to the tensile direction. Conversely, the specimens printed with their layer direction parallel to the tensile direction presented a low ultimate strength and low strain at breakage. The fact that the specimens with their layer direction parallel to the tensile direction presented a low ultimate strength and low strain at breakage is a usual behavior of parts obtained by means of FDM. The SEM images revealed oriented binder domains in the printed parts and oriented voids in the sintered parts. It was assumed that large binder domains in the filament were oriented perpendicular to the layer directions during the fused deposition modeling printing, and remained as oriented voids after sintering. Stress concentration in the oriented void defects was likely responsible for the poor tensile properties of these specimens.
17-4PH不锈钢试样采用金属熔融沉积(FDMet)技术制造,该技术将17-4PH颗粒与有机粘结剂结合在一起。FDMet有望成为一种低成本的增材制造工艺。本研究旨在阐明3D打印过程中层方向对烧结态和时效态试样的力学性能和收缩性能的影响。所有试样(在三个层方向上打印的烧结态和时效态试样)均表现出较高的相对密度(97.5-98%)。当层方向垂直于拉伸方向时,获得了最高的极限强度(烧结态和时效态试样分别为880和1140MPa)。相反,层方向平行于拉伸方向打印的试样呈现出较低的极限强度和断裂应变。层方向平行于拉伸方向的试样呈现出较低的极限强度和断裂应变这一事实是通过熔融沉积成型(FDM)获得的零件的常见行为。扫描电子显微镜(SEM)图像显示了打印零件中取向的粘结剂区域和烧结零件中取向的孔隙。据推测,在熔融沉积建模打印过程中,长丝中的大粘结剂区域垂直于层方向取向,并在烧结后保留为取向孔隙。取向孔隙缺陷中的应力集中可能是这些试样拉伸性能较差的原因。