Institute of Physical Metallurgy, Metalforming and Nanotechnology, University of Miskolc, Hungary.
Faculty of Engineering, Al-Qasim Green University, Al-Qasim/Babylon, Iraq.
Sci Prog. 2023 Jan-Mar;106(1):368504221146060. doi: 10.1177/00368504221146060.
The press and sinter method remains the standard among powder metallurgy processes for powdered stainless-steel materials. It delivers low cost, low oxidation rate, and adequate corrosion resistance. Furthermore, 17-4PH is a martensitic stainless-steel that is commonly used for high-strength and medium-ductility stainless steel parts. However, a few studies have investigated the press and sinter method for producing 17-4PH parts. This shortage is due to the high hardness (low compressibility) of 17-4PH powder. Thus, the main objective of this study is to evaluate the press and sinter method in terms of the manufacturing process, the influencing factors, and the theoretical basis of press and sinter methods in conjunction with metal injection molding technology for the production of 17-4PH parts. First, the literature and monographs are examined and summarized to cover the previous results, research progress, development trends, and applications of press and sinter method 17-4PH parts. Following the theoretical analysis, the practical investigation was conducted by producing parts with cold pressing from 800 to 1600 MPa, followed by sintering: the sintering temperature was 1200 °C for one hour under a protective vacuum atmosphere. ImageJ analysis was performed to measure the sinter density. The results showed an increase in relative sinter density from 84.43% to 96.43% for 800 and 1600 MPa, respectively, while the earlier results reached 93.47%. Overall, the press and sinter method enables the production of high-hardness 17-4PH parts with a high density, without using additives like lubricants, wax, or alloying elements.
粉末冶金工艺中,压制和烧结法仍然是粉末不锈钢材料的标准工艺。它具有成本低、氧化率低和足够的耐腐蚀性等优点。此外,17-4PH 是一种马氏体不锈钢,常用于高强度和中等延展性的不锈钢零件。然而,很少有研究探讨过压制和烧结法生产 17-4PH 零件。这是由于 17-4PH 粉末的硬度高(可压缩性低)。因此,本研究的主要目的是评估压制和烧结法在制造工艺、影响因素以及与金属注射成型技术相结合的压制和烧结法理论基础方面,用于生产 17-4PH 零件。首先,通过查阅文献和专著,对压制和烧结法生产 17-4PH 零件的先前结果、研究进展、发展趋势和应用进行了综述和总结。在理论分析之后,通过冷压从 800 到 1600 MPa 来生产零件,并进行烧结:在保护真空气氛下,烧结温度为 1200°C 一小时。使用 ImageJ 分析来测量烧结密度。结果表明,800 和 1600 MPa 下的相对烧结密度分别从 84.43%增加到 96.43%,而早期的结果达到了 93.47%。总体而言,压制和烧结法能够生产出高密度的高硬度 17-4PH 零件,而无需使用润滑剂、蜡或合金元素等添加剂。