Int J Prosthodont. 2021 November/December;34(6):763–774. doi: 10.11607/ijp.6992. Epub 2021 Feb 12.
To evaluate the failure load of 3D-printed denture resin material and teeth before and after dynamic loading.
A total of 40 specimens were fabricated following ISO/TS 19736 and were divided into two equal groups. In the test group, the cylindrical base and denture teeth were 3D printed separately and then luted together. In the control group, the specimens were fabricated from conventional heat-cured polymethyl methacrylate (PMMA) and commercially available denture teeth using the compression-molding technique. Ten specimens from each group were subjected to dynamic load of 50 N for 250,000 cycles in a chewing simulator. All specimens were subjected to static load of 50 N using Instron machine with a crosshead speed of 1 mm/minute until fracture. The fractured surfaces were analyzed using field emission scanning electron microscopy. The failure loads were calculated and compared using analysis of variance (P < .05).
All specimens survived the loading, undergoing 250,000 cycles without fracture. The mean failure load was influenced by fabrication technique and was significantly higher for the 3D-printed test group (P = .028). 3D-printed teeth showed a mixed mode of fracture, whereas in the control group, the specimens showed cohesive fracture within the teeth.
The fabrication technique has an influence on the mode of failure between acrylic teeth and resin base material. Cohesive failure in teeth was predominant in the conventional group, suggesting possibly higher bond strength between the teeth and resin base in this group. The observed failure modes reveal that both fabrication techniques exhibited satisfactory bond strength. Chewing simulation did not significantly influence the bond strength of any of the tested groups.
评估 3D 打印义齿树脂材料和牙齿在动态加载前后的失效负荷。
根据 ISO/TS 19736 标准共制作 40 个试件,分为两组,每组 20 个。实验组的圆柱形基底和义齿牙分别 3D 打印,然后粘在一起。对照组的试件由传统热固性聚甲基丙烯酸甲酯(PMMA)和市售义齿牙通过压缩成型技术制成。每组 10 个试件在咀嚼模拟器中以 50N 的动态载荷进行 25 万次循环。所有试件均在 Instron 机器上以 1mm/min 的十字头速度施加 50N 的静态载荷直至断裂。使用场发射扫描电子显微镜分析断裂面。使用方差分析(P <.05)计算并比较失效载荷。
所有试件均经受住了 25 万次循环的加载而未发生断裂。失效负荷受制作技术影响,3D 打印实验组显著更高(P =.028)。3D 打印牙显示混合断裂模式,而对照组试件显示牙内的内聚性断裂。
制作技术对义齿牙和树脂基底材料之间的失效模式有影响。在传统组中,牙内的内聚性断裂占主导地位,这表明该组中牙与树脂基底之间可能具有更高的结合强度。观察到的失效模式表明,两种制作技术均表现出令人满意的结合强度。咀嚼模拟对任何测试组的结合强度均无显著影响。