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欧洲X射线自由电子激光装置上用于小量子系统仪器的100万像素pnCCD探测器:系统与运行方面

The 1-Megapixel pnCCD detector for the Small Quantum Systems Instrument at the European XFEL: system and operation aspects.

作者信息

Kuster Markus, Ahmed Karim, Ballak Kai Erik, Danilevski Cyril, Ekmedžić Marko, Fernandes Bruno, Gessler Patrick, Hartmann Robert, Hauf Steffen, Holl Peter, Meyer Michael, Montaño Jacobo, Münnich Astrid, Ovcharenko Yevheniy, Rennhack Nils, Rüter Tonn, Rupp Daniela, Schlosser Dieter, Setoodehnia Kiana, Schmitt Rüdiger, Strüder Lothar, Tanyag Rico Mayro P, Ulmer Anatoli, Yousef Hazem

机构信息

European XFEL, Holzkoppel 4, 22869 Schenefeld, Germany.

PNSensor GmbH, Otto-Hahn-Ring 6, 81739 München, Germany.

出版信息

J Synchrotron Radiat. 2021 Mar 1;28(Pt 2):576-587. doi: 10.1107/S1600577520015659. Epub 2021 Jan 28.

Abstract

The X-ray free-electron lasers that became available during the last decade, like the European XFEL (EuXFEL), place high demands on their instrumentation. Especially at low photon energies below 1 keV, detectors with high sensitivity, and consequently low noise and high quantum efficiency, are required to enable facility users to fully exploit the scientific potential of the photon source. A 1-Megapixel pnCCD detector with a 1024 × 1024 pixel format has been installed and commissioned for imaging applications at the Nano-Sized Quantum System (NQS) station of the Small Quantum System (SQS) instrument at EuXFEL. The instrument is currently operating in the energy range between 0.5 and 3 keV and the NQS station is designed for investigations of the interaction of intense FEL pulses with clusters, nano-particles and small bio-molecules, by combining photo-ion and photo-electron spectroscopy with coherent diffraction imaging techniques. The core of the imaging detector is a pn-type charge coupled device (pnCCD) with a pixel pitch of 75 µm × 75 µm. Depending on the experimental scenario, the pnCCD enables imaging of single photons thanks to its very low electronic noise of 3 e and high quantum efficiency. Here an overview on the EuXFEL pnCCD detector and the results from the commissioning and first user operation at the SQS experiment in June 2019 are presented. The detailed descriptions of the detector design and capabilities, its implementation at EuXFEL both mechanically and from the controls side as well as important data correction steps aim to provide useful background for users planning and analyzing experiments at EuXFEL and may serve as a benchmark for comparing and planning future endstations at other FELs.

摘要

过去十年间出现的X射线自由电子激光器,如欧洲X射线自由电子激光器(EuXFEL),对其仪器设备有很高的要求。特别是在低于1千电子伏特的低光子能量下,需要具有高灵敏度、因此低噪声和高量子效率的探测器,以使设施用户能够充分利用光子源的科学潜力。一个1024×1024像素格式的100万像素pnCCD探测器已安装并调试,用于EuXFEL的小量子系统(SQS)仪器的纳米尺寸量子系统(NQS)站的成像应用。该仪器目前在0.5至3千电子伏特的能量范围内运行,NQS站旨在通过将光离子和光电子能谱与相干衍射成像技术相结合,研究强自由电子激光脉冲与团簇、纳米颗粒和小生物分子的相互作用。成像探测器的核心是一个像素间距为75微米×75微米的pn型电荷耦合器件(pnCCD)。根据实验场景,pnCCD因其3电子的极低电子噪声和高量子效率,能够对单光子进行成像。本文介绍了EuXFEL pnCCD探测器的概况以及2019年6月在SQS实验中的调试结果和首次用户操作情况。对探测器设计和功能、其在EuXFEL的机械和控制方面的实现以及重要的数据校正步骤的详细描述,旨在为计划和分析EuXFEL实验的用户提供有用的背景信息,并可作为比较和规划其他自由电子激光未来终端站的基准。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/f7db/7941295/9b189842283d/s-28-00576-fig1.jpg

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