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柠檬草(Cymbopogon citratus DC. Stapf)精油微球的制备、表征及抗氧化活性研究。

Lemongrass (Cymbopogon citratus DC. Stapf) essential oil microparticles: Development, characterization, and antioxidant potential.

机构信息

Center for Agro-Food Science and Technology, Federal University of Campina Grande, Pombal, Paraíba, Brazil.

Department of Organic and Inorganic Chemistry, Federal University of Ceará, Fortaleza, Ceará, Brazil.

出版信息

Food Chem. 2021 Sep 1;355:129644. doi: 10.1016/j.foodchem.2021.129644. Epub 2021 Mar 22.

Abstract

Maltodextrin (DE 20) and gelatin (4:1, w/w, respectively) were investigated as encapsulant materials for lemongrass (Cymbopogon citratus DC. Stapf) essential oil microencapsulation by freeze-drying. Three formulations were prepared: M (5% essential oil), M (10% essential oil), and M (15% essential oil), all in w/w. Microparticles were characterized by Fourier-transform infrared spectroscopy, scanning electron microscopy, water activity measurement, thermogravimetric and derivative thermogravimetric analysis, differential scanning calorimetry, and antioxidant activity analysis. Yield and microencapsulation efficiency were also determined. The results showed the promising potential of maltodextrin and gelatin as encapsulants and confirmed the feasibility of preparing C. citratus essential oil microparticles by freeze-drying. Microencapsulation improved the oil's thermal and oxidative stability, providing protection from volatilization and environmental conditions. Scanning electron microscopic examination of M revealed a closed, pore-free surface. M had higher yield and microencapsulation efficiency, showing great commercial potential for its reduced storage, transport, and distribution costs.

摘要

麦芽糊精(DE20)和明胶(分别为 4:1,w/w)被研究用作柠檬草(Cymbopogon citratus DC. Stapf)精油微胶囊冷冻干燥的包埋材料。制备了三种配方:M(5%精油)、M(10%精油)和 M(15%精油),均为 w/w。通过傅里叶变换红外光谱、扫描电子显微镜、水分活度测量、热重和导数热重分析、差示扫描量热法和抗氧化活性分析对微粒子进行了表征。还测定了产率和微胶囊化效率。结果表明,麦芽糊精和明胶具有作为包埋剂的巨大潜力,并证实了通过冷冻干燥制备柠檬草精油微粒子的可行性。微胶囊化提高了油的热稳定性和抗氧化稳定性,提供了对挥发和环境条件的保护。M 的扫描电子显微镜检查显示出封闭的、无孔的表面。M 具有更高的产率和微胶囊化效率,由于其降低了储存、运输和分销成本,具有巨大的商业潜力。

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