de Oliveira Alencar Denise Dantas, de Souza Evandro Leite, da Cruz Almeida Erika Thayse, da Silva André Leandro, Oliveira Hugo Miguel Lisboa, Cavalcanti Mônica Tejo
Post-Graduation Program in Agroindustrial Systems, Center for Agro-Food Science and Technology, Federal University of Campina Grande, Pombal 58840-000, PB, Brazil.
Laboratory of Food Microbiology, Department of Nutrition, Health Sciences Center, Federal University of Paraíba, João Pessoa 58051-900, PB, Brazil.
Foods. 2022 Apr 13;11(8):1111. doi: 10.3390/foods11081111.
This study aimed to microencapsulate essential oil (CCEO) with spray drying using maltodextrin and gelatin. The effects of the operational conditions (inlet temperature (130-160 °C), CCEO concentration (5-15%), maltodextrin concentration (10-20%)) on the physicochemical stability and antioxidant and antibacterial activities of the CCEO microcapsules were determined. The CCEO microencapsulation process had yield and encapsulation efficiency values varying from 31.02 to 77.53% and 15.86-61.95%, respectively. CCEO microcapsules had antibacterial effects against and with minimum inhibitory concentration varying from 10 to 20%, and total phenolic contents and antioxidant activities varying from 1632 to 4171.08 μg TE/g and 28.55-45.12 µg/g, respectively. CCEO microcapsules had average diameters varying from 5.10 to 10.11 µm, with spherical external structures without cracks and apparent pores. The best desirable process conditions for CCEO microencapsulation were process inlet temperature of 148 °C, maltodextrin concentration of 15%, and CCEO concentration of 10%. The results showed that CCEO microcapsules with increased stability and low degradation of active components can be prepared by spray drying using maltodextrin and gelatin with the production of microcapsules, which could be exploited as potential food preservatives.
本研究旨在使用麦芽糊精和明胶通过喷雾干燥法对香蜂草精油(CCEO)进行微胶囊化。测定了操作条件(进样温度(130 - 160℃)、CCEO浓度(5 - 15%)、麦芽糊精浓度(10 - 20%))对CCEO微胶囊物理化学稳定性、抗氧化和抗菌活性的影响。CCEO微胶囊化过程的产率和包封率分别在31.02%至77.53%和15.86 - 61.95%之间变化。CCEO微胶囊对[具体菌种1]和[具体菌种2]有抗菌作用,最低抑菌浓度在10%至20%之间,总酚含量和抗氧化活性分别在1632至4171.08 μg TE/g和28.55 - 45.12 µg/g之间。CCEO微胶囊的平均直径在5.10至10.11 µm之间,具有球形外部结构,无裂缝和明显孔隙。CCEO微胶囊化的最佳工艺条件为进样温度148℃、麦芽糊精浓度15%、CCEO浓度10%。结果表明,使用麦芽糊精和明胶通过喷雾干燥法可制备出稳定性增强且活性成分降解率低的CCEO微胶囊,这些微胶囊可作为潜在的食品防腐剂加以利用。