Burkhardt Felix, Harlass Markus, Adolfsson Erik, Vach Kirstin, Spies Benedikt Christopher, Kohal Ralf-Joachim
Medical Center-University of Freiburg, Center for Dental Medicine, Department of Prosthetic Dentistry, Faculty of Medicine, University of Freiburg, Hugstetter Str. 55, 79106 Freiburg, Germany.
Swerea IVF AB, Argongatan 30, 431 53 Mölndal, Sweden.
Materials (Basel). 2021 Apr 23;14(9):2151. doi: 10.3390/ma14092151.
A novel ceria-stabilized zirconia-alumina-aluminate composite (Ce-TZP-comp) that is not prone to aging presents a potential alternative to yttrium-stabilized zirconia for ceramic oral implants. The objective of this study was to evaluate the long-term stability of a one-piece narrow-diameter implant made of Ce-TZP-comp. Implant prototypes with a narrow (3.4 mm) and regular (4.0 mm) diameter were embedded according to ISO 14801, and subgroups (n = 8) were subsequently exposed to dynamic loading (10 cycles, 98N) and/or hydrothermal treatment (aging, 85 °C). Loading/aging was only applied as a combined protocol for the 4.0 mm diameter implants. One subgroup of each diameter remained untreated. One sample was cross-sectioned from each subgroup and evaluated with a scanning electron microscope for phase-transformation of the lattice. Finally, the remaining samples were loaded to fracture. A multivariate linear regression model was applied for statistical analyses (significance at < 0.05). All samples withstood the different loading/aging protocols and no transformation propagation was observed. The narrow diameter implants showed the lowest fracture load after combined loading/aging (628 ± 56 N; < 0.01), whereas all other subgroups exhibited no significantly reduced fracture resistance (between 762 ± 62 and 806 ± 73 N; > 0.05). Therefore, fracture load values of Ce-TZP-comp implants suggest a reliable intraoral clinical application in the anterior jaw regions.
一种不易老化的新型二氧化铈稳定的氧化锆-氧化铝-铝酸盐复合材料(Ce-TZP-comp)为陶瓷口腔种植体提供了一种替代钇稳定氧化锆的潜在选择。本研究的目的是评估由Ce-TZP-comp制成的一体式窄直径种植体的长期稳定性。根据ISO 14801将窄直径(3.4 mm)和常规直径(4.0 mm)的种植体原型植入,随后将亚组(n = 8)暴露于动态加载(10个循环,98N)和/或水热处理(老化,85°C)。加载/老化仅作为4.0 mm直径种植体的联合方案应用。每个直径的一个亚组保持未处理状态。从每个亚组中取一个样本进行横截面切片,并用扫描电子显微镜评估晶格的相变。最后,将剩余的样本加载至断裂。应用多元线性回归模型进行统计分析(显著性水平<0.05)。所有样本均能承受不同的加载/老化方案,未观察到相变扩展。窄直径种植体在联合加载/老化后显示出最低的断裂载荷(628±56 N;<0.01),而所有其他亚组的抗断裂性均未显著降低(762±62至806±73 N之间;>0.05)。因此,Ce-TZP-comp种植体的断裂载荷值表明其在前牙区的口腔内临床应用是可靠的。