Nino-Barrera Javier, Sanchez-Aleman Jose, Acosta-Humanez Manuel, Gamboa-Martinez Luis, Cortes-Rodriguez Carlos
Faculty of Dentistry, Endodontics Program, Universidad Nacional de Colombia, Building 210, Office 301, Bogotá, Colombia.
Department of Physics, Universidad Nacional de Colombia, Bogotá, Colombia.
Sci Rep. 2021 Jun 21;11(1):12961. doi: 10.1038/s41598-021-92382-x.
The objective of this study was to assess the resistance to fatigue fracture of conventional nickel-titanium files after undergoing shot peening. Forty NITIFLEX endodontic files, number 30, were divided into two groups; one was submitted to shot peening treatment and the other was not. All instruments were tested for fatigue fracture in simulated canals with a TRI-AUTO ZX endodontic motor. One file of each group was subjected to a residual stress analysis by XRD. Finally, the fractured surface was observed and elemental analysis performed by means of SEM and EDX. Roughness analysis was made by focal variation microscope. The shot peening group showed greater resistance to fatigue fracture; there was no difference in the length of the fractured fragments. XRD results showed the presence of residual compression stresses in the file submitted to shot peening, a decrease in the interplanar spacing, and an increase in the full-width-at-half-maximum and the microstrains. SEM and EDX showed a ductile fracture with zones of fatigue and an equiatomic ratio between the nickel and titanium. Surface roughness increased after the file was subjected to the shot peening procedure. In conclusion, shot peening increases the resistance to fatigue fracture due to the presence of residual compression stresses in files manufactured from a conventional nickel-titanium alloy.
本研究的目的是评估经喷丸处理后的传统镍钛锉的抗疲劳断裂性能。40根30号的NITIFLEX根管锉被分为两组;一组进行喷丸处理,另一组不进行处理。所有器械均使用TRI-AUTO ZX根管马达在模拟根管中进行疲劳断裂测试。每组取一根锉进行X射线衍射(XRD)残余应力分析。最后,观察断裂表面,并通过扫描电子显微镜(SEM)和能谱仪(EDX)进行元素分析。使用聚焦变化显微镜进行粗糙度分析。喷丸处理组显示出更高的抗疲劳断裂性能;断裂碎片的长度没有差异。XRD结果表明,经喷丸处理的锉中存在残余压应力,晶面间距减小,半高宽和微观应变增加。SEM和EDX显示为韧性断裂,伴有疲劳区域,镍和钛的原子比相等。锉经喷丸处理后表面粗糙度增加。总之,由于传统镍钛合金制造的锉中存在残余压应力,喷丸处理提高了其抗疲劳断裂性能。