Health Science Center, Department of Dentistry, Division of Prosthodontics, Federal University of Rio Grande Do Norte (UFRN), Avenida Senador Salgado Filho, nº 1787, Lagoa Nova, Natal, RN, 59056-000, Brazil.
Department of Dentistry, University of Pernambuco (UPE), Av. Governador Agamenon Magalhães, S/N- Santo Amaro, Recife, PE, 50100-010, Brazil.
Clin Oral Investig. 2022 Jan;26(1):889-900. doi: 10.1007/s00784-021-04068-3. Epub 2021 Aug 27.
To investigate the influence of different finishing/polishing techniques and in situ aging on the flexural strength (σ), surface roughness, and Candida albicans adherence of 5 mol% yttria-stabilized zirconia (ultratranslucent zirconia).
A total of 120 zirconia bars (Prettau Anterior, Zirkonzahn) with dimensions of 8 × 2 × 0.5 mm were divided into 8 groups (n = 15) according to two factors: "in situ aging" (non-aged and aged (A)) and "finishing/polishing" (control (C), diamond rubber polishing (R), coarse grit diamond bur abrasion (B), and coarse grit diamond bur abrasion + diamond rubber polishing (BR)). Half of the samples from each group were subjected to a 60-day in situ aging by fixing the bars into cavities prepared in the posterior region of the base of complete or partial dentures of 15 patients. The samples were then subjected to the mini flexural (σ) test (1 mm/min). A total of 40 zirconia blocks (5 × 5 × 2 mm) were prepared and subjected to roughness (Ra) analyses and fungal adherence and complementary analyses (X-ray diffraction (XRD) and scanning electron microscopy (SEM)). The data of mean σ (MPa) and roughness Ra (μm) were statistically analyzed by two-way and one-way ANOVA, respectively, and Tukey's test. The Weibull analysis was performed for σ data. The fungal adhesion (Log CFU/mL) data were analyzed by Kruskal-Wallis tests.
For flexural resistance, the "finishing/polishing" factor was statistically significant (P = 0.0001); however, the "in situ aging" factor (P = 0.4458) was not significant. The non-aged (507.3 ± 115.7 MPa) and aged (487.6 ± 118.4 MPa) rubber polishing groups exhibited higher mean σ than the other techniques. The non-aged (260.2 ± 43.3 MPa) and aged (270.1 ± 48.8 MPa) bur abrasion groups presented lower σ. The coarse-grit diamond bur abrasion group (1.82 ± 0.61 µm) presented the highest roughness value (P = 0.001). Cell adhesion was not different among groups (P = 0.053). Group B presented the most irregular surface and the highest roughness Ra of 0.61 m.
The finishing of ultratranslucent zirconia might be preferably done with a diamond rubber polisher. Moreover, the protocols used did not interfere with Candida albicans adhesion.
Coarse-grit diamond burs might be avoided for finishing ultratranslucent monolithic zirconia, which might be preferably performed with a diamond rubber polisher.
研究不同的修整/抛光技术以及原位老化对 5mol%氧化钇稳定氧化锆(超透明氧化锆)的弯曲强度(σ)、表面粗糙度和白色念珠菌黏附的影响。
共 120 个 Prettau Anterior(Zirkonzahn)氧化锆棒(8×2×0.5mm)根据两个因素分为 8 组(n=15):“原位老化”(未老化和老化(A))和“修整/抛光”(对照(C)、金刚石橡胶抛光(R)、粗粒度金刚石车削磨损(B)和粗粒度金刚石车削磨损+金刚石橡胶抛光(BR))。每组的一半样本在 15 名患者的全口或局部义齿基底部后区制备的腔中固定棒后,进行为期 60 天的原位老化。然后对样本进行微型弯曲(σ)测试(1mm/min)。共制备 40 个氧化锆块(5×5×2mm),进行粗糙度(Ra)分析和真菌黏附及补充分析(X 射线衍射(XRD)和扫描电子显微镜(SEM))。用双向和单向方差分析分别对平均 σ(MPa)和粗糙度 Ra(μm)数据进行统计学分析,并用 Tukey 检验进行比较。对 σ 数据进行威布尔分析。用 Kruskal-Wallis 检验分析真菌黏附(Log CFU/mL)数据。
对于弯曲强度,“修整/抛光”因素具有统计学意义(P=0.0001);然而,“原位老化”因素(P=0.4458)无统计学意义。未老化(507.3±115.7MPa)和老化(487.6±118.4MPa)橡胶抛光组的平均 σ 值高于其他技术。未老化(260.2±43.3MPa)和老化(270.1±48.8MPa)车削磨损组的 σ 值较低。粗粒度金刚石车削磨损组(1.82±0.61μm)呈现出最高的粗糙度值(P=0.001)。各组间细胞黏附无差异(P=0.053)。B 组表面最不规则,Ra 最高,为 0.61μm。
超透明氧化锆的修整最好使用金刚石橡胶抛光器。此外,所用方案不影响白色念珠菌黏附。
打磨超透明整体氧化锆时,可能最好避免使用粗粒度金刚石车削,而使用金刚石橡胶抛光器。