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用于CAD/CAM应用的可打印和可加工牙科修复复合材料——力学性能、断口形貌、纹理和分形维数分析的比较

Printable and Machinable Dental Restorative Composites for CAD/CAM Application-Comparison of Mechanical Properties, Fractographic, Texture and Fractal Dimension Analysis.

作者信息

Grzebieluch Wojciech, Kowalewski Piotr, Grygier Dominika, Rutkowska-Gorczyca Małgorzata, Kozakiewicz Marcin, Jurczyszyn Kamil

机构信息

Laboratory for Digital Dentistry, Department of Conservative Dentistry Witch Endodontics, Wroclaw Medical University, Krakowska 26, 50-425 Wroclaw, Poland.

Department of Fundamentals of Machine Design and Mechatronic Systems, Wroclaw University of Science and Technology, Lukasiewicza 7/9, 50-371 Wroclaw, Poland.

出版信息

Materials (Basel). 2021 Aug 29;14(17):4919. doi: 10.3390/ma14174919.

DOI:10.3390/ma14174919
PMID:34501009
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC8434230/
Abstract

Thanks to the continuous development of light-curing resin composites it is now possible to print permanent single-tooth restorations. The purpose of this study was to compare resin composites for milling -Gandio Blocks (GR), Brilliant Crios (CR) and Enamic (EN) with resin composite for 3D printing-Varseo Smile Crown plus (VSC). Three-point bending was used to measure flexural strength (σ) and flexural modulus (E). The microhardness was measured using a Vickers method, while fractographic, microstructural, texture and fractal dimension (FD) analyses were performed using SEM, optical microscope and picture analysis methods. The values of σ ranged from 118.96 (±2.81) MPa for EN to 186.02 (±10.49) MPa for GR, and the values of E ranged from 4.37 (±0.8) GPa for VSC to 28.55 (±0.34) GPa for EN. HV01 ranged from 25.8 (±0.7) for VSC to 273.42 (±27.11) for EN. The filler content ranged from 19-24 vol. % for VSC to 70-80 vol. % for GR and EN. The observed fractures are typical for brittle materials. The correlation between FD of materials microstructure and E was observed. σ of the printed resin depends on layers orientation and is significantly lower than σ of GR and CR. E of the printed material is significantly lower than E of blocks for milling.

摘要

得益于光固化树脂复合材料的不断发展,现在已经能够打印永久性单颗牙齿修复体。本研究的目的是比较用于铣削的树脂复合材料——甘迪奥块体(GR)、辉煌克里奥斯(CR)和伊纳米克(EN)与用于3D打印的树脂复合材料——瓦尔塞奥微笑冠加(VSC)。采用三点弯曲法测量弯曲强度(σ)和弯曲模量(E)。使用维氏方法测量显微硬度,同时使用扫描电子显微镜、光学显微镜和图像分析方法进行断口分析、微观结构分析、纹理分析和分形维数(FD)分析。σ的值范围为EN的118.96(±2.81)MPa至GR的186.02(±10.49)MPa,E的值范围为VSC的4.37(±0.8)GPa至EN的28.55(±0.34)GPa。HV01的值范围为VSC的25.8(±0.7)至EN的273.42(±27.11)。填料含量范围为VSC的19 - 24体积%至GR和EN的70 - 80体积%。观察到的断裂是脆性材料的典型特征。观察到材料微观结构的FD与E之间存在相关性。打印树脂的σ取决于层的取向,并且显著低于GR和CR的σ。打印材料的E显著低于用于铣削的块体的E。

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