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电子鼻技术在基于纯度和白砂糖百分比预测甘蔗糖浆质量方面的应用。

Application of E-nose technique to predict sugarcane syrup quality based on purity and refined sugar percentage.

作者信息

Zaki Dizaji Hassan, Adibzadeh Abdullah, Aghili Nategh Nahid

机构信息

Department of Biosystems Engineering, Faculty of Agriculture, Shahid Chamran University of Ahvaz, Ahvaz, Iran.

Department of Agricultural Machinery Engineering, Sonqor Agriculture Faculty, Razi University, Kermanshah, Iran.

出版信息

J Food Sci Technol. 2021 Nov;58(11):4149-4156. doi: 10.1007/s13197-020-04879-4. Epub 2020 Nov 4.

Abstract

Rapid test methods with portable devices along with standard chemical tests are necessary to determine raw syrup quality in the sugarcane agro-industries. On this account, a special e-nose device was developed to test the sugarcane syrup and its association with the odor emitted from it to determine the amount of sucrose (purity) in the sugarcane syrup. Samples were obtained from the farms of Hakim-Farabi agro-industry, including four varieties (CP57, CP69, IRC99-02, and CP48). Experiments included chemical tests to determine the percentage of purity (PTY) and refined sugar (RS) plus an electronic nose test. Partial least squares (PLS), principle component regression (PCR), multiple linear regression (MLR), and artificial neural network (ANN) methods were used to evaluate the correlation between the gained signals from the sensor array and chemical analysis results of the samples. In the case of PTY, among 8 sensors, MQ3, MQ5, and MQ9 had the highest response compared to the others, while regarding RS, all the sensors except for MQ8 indicated a great contribution. Also, all models for PTY and RS showed a good prediction performance. The results revealed that ANN model, with topology 8-1-2, outperformed others for prediction of the quality indices of sugarcane, with high correlation coefficients (R = 0.96 for RS; 0.99 for PTY), and relatively low RMSE values of 0.33 for RS; 0.4 for RTY. Finally, findings indicated that e-nose technique has the potential to become an authentic tool to assess chemical features of sugarcane syrup from e-nose system signals.

摘要

在甘蔗农工业中,使用便携式设备的快速检测方法以及标准化学检测对于确定原糖浆质量是必要的。基于此,开发了一种特殊的电子鼻设备来检测甘蔗糖浆及其散发的气味,以确定甘蔗糖浆中蔗糖的含量(纯度)。样本取自哈基姆 - 法拉比农工业的农场,包括四个品种(CP57、CP69、IRC99 - 02和CP48)。实验包括用于确定纯度百分比(PTY)和精制糖(RS)的化学检测以及电子鼻检测。使用偏最小二乘法(PLS)、主成分回归(PCR)、多元线性回归(MLR)和人工神经网络(ANN)方法来评估传感器阵列获得的信号与样本化学分析结果之间的相关性。对于PTY,在8个传感器中,MQ3、MQ5和MQ9与其他传感器相比具有最高的响应,而对于RS,除MQ8外的所有传感器都显示出很大的贡献。此外,所有关于PTY和RS的模型都显示出良好的预测性能。结果表明,拓扑结构为8 - 1 - 2的ANN模型在预测甘蔗质量指标方面优于其他模型,相关系数较高(RS为0.96;PTY为0.99),RS的RMSE值相对较低,为0.33;RTY为0.4。最后,研究结果表明,电子鼻技术有潜力成为一种根据电子鼻系统信号评估甘蔗糖浆化学特征的可靠工具。

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A 21st century technique for food control: electronic noses.一种21世纪的食品控制技术:电子鼻。
Anal Chim Acta. 2009 Apr 6;638(1):1-15. doi: 10.1016/j.aca.2009.02.009. Epub 2009 Feb 12.

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