Comparative evaluation of the effect of thermocycling on the mechanical properties of conventionally polymerized, CAD-CAM milled, and 3D-printed interim materials.

STATEMENT OF PROBLEM

Studies on the energy absorption characteristics by means of elastic and plastic material deformation of interim materials are lacking.

PURPOSE

The purpose of this in vitro study was to compare the effect of different thermocycling periods on the flexural strength (σ), resilience (U), and toughness (U) of conventionally polymerized, computer-aided design and computer-aided manufacturing (CAD-CAM) milled, and 3-dimensionally (3D) printed interim materials.

MATERIAL AND METHODS

Rectangular specimens (n=30 for each material) were fabricated from autopolymerized polymethyl methacrylate (PMMA), bis-acryl resin (Bis-acryl), CAD-CAM polymethyl methacrylate-based polymer (CAD-CAM/Milled), and 3D-printed composite resin (3D-Printed). Each material was divided into 3 groups (n=10) according to the applied thermocycling (5 °C to 55 °C) procedure: control (0 cycles), 2500, and 10 000 cycles. Parameters of the materials such as σ, U, and U were tested in a 3-point bend test according to International Organization for Standardization (ISO) 10477. Data were statistically analyzed with the Shapiro-Wilk test followed by Kruskal-Wallis test, the Mann-Whitney U test, the Friedman test, and Wilcoxon signed-rank test (α=.05).

RESULTS

The tested material and thermocycling had a statistically significant influence on the σ, U, and U values (P<.05). PMMA showed the lowest mean σ, U, and U values (P<.05), and CAD-CAM/Milled showed σ values similar to those of 3D-Printed at all thermocycling periods. CAD-CAM/Milled showed the highest U values at 10 000 cycles and the highest U values at all thermocycles. No significant differences were found in the mean change of σ and U of CAD-CAM/Milled among different thermocycling periods.

CONCLUSIONS

The results suggested that digitally fabricated interim materials had better mechanical properties than conventionally polymerized materials and that milled materials had the highest stability in maintaining their initial capacity to absorb energy.