Dipartimento di Scienza e Tecnologia del Farmaco, Università degli Studi di Torino, Torino, Italy.
J Sep Sci. 2022 Jan;45(1):94-112. doi: 10.1002/jssc.202100681.
This review is an overview of the recent advances of gas chromatography in essential oil analysis; in particular, it focuses on both the new stationary phases and the advanced analytical methods and instrumentations. A paragraph is dedicated to ionic liquids as gas chromatography stationary phases, showing that, thanks to their peculiar selectivity, they can offer a complementary contribution to conventional stationary phases for the analysis of complex essential oils and the separation of critical pairs of components. Strategies to speed-up the analysis time, thus answering to the ever increasing request for routine essential oils quality control, are also discussed. Last but not least, a paragraph is dedicated to recent developments in column miniaturization in particular that based on microelectromechanical-system technology in a perspective of developing micro-gas chromatographic systems to optimize the energy consumption as well as the instrumentation dimensions. A number of applications in the essential oil field is also included.
这篇综述概述了气相色谱在精油分析中的最新进展;特别是,它侧重于新的固定相以及先进的分析方法和仪器。还有一个段落专门介绍了离子液体作为气相色谱固定相,表明由于其特殊的选择性,它们可以为分析复杂精油和分离关键成分对提供常规固定相的补充。还讨论了加速分析时间的策略,以满足对常规精油质量控制的需求不断增加。最后但同样重要的是,还有一个段落专门介绍了柱微型化的最新进展,特别是基于微机电系统技术的进展,旨在开发微气相色谱系统以优化能量消耗和仪器尺寸。还包括一些在精油领域的应用。