Opatragoon Suphakit, Klaisiri Awiruth, Sriamporn Tool, Thamrongananskul Niyom
Department of Prosthodontics, Faculty of Dentistry, Chulalongkorn University, Bangkok, Thailand.
Division of Restorative Dentistry, Faculty of Dentistry, Thammasat University, Pathum Thani, Thailand.
Eur J Dent. 2024 Oct;18(4):1004-1011. doi: 10.1055/s-0043-1777821. Epub 2024 Jul 16.
This study examined the effect of the number of phosphate-containing primer applications on the shear bond strength (SBS) of zirconia to resin cement.
315 square specimens (10 × 10 × 4 mm) were manufactured from Cercon ht presintered zirconia blocks. Alumina particles were used to sandblast zirconia specimens. These specimens were randomly divided into six primer-based groups: No primer application (NP), CLEARFIL CERAMIC PRIMER (C), PANAVIA V5 Tooth Primer (T), M&C PRIMER (MC), Monobond N (MN), and Z-PRIME plus (Z), and then separated into application number (1-4) groups (excluding NP). Each specimen was bonded with resin cement. The SBS was measured using a universal testing machine. The debonded surface was examined with a stereomicroscope.
The SBSs were analyzed using two-way analysis of variance.
Applying the primer twice exhibited the highest SBSs in each group, with significant differences in the T, MN, and Z groups. However, the SBS in the MC group was significantly lower on the second application. One-hundred percent adhesive failure was observed in all groups.
Within the limitations of this study, prior to cementation, the sandblasted zirconia surface should be applied twice with a phosphate-containing primer other than MC to maximize the SBS at the zirconia-resin cement interface.
本研究考察了含磷酸盐底漆涂抹次数对氧化锆与树脂水门汀之间剪切粘结强度(SBS)的影响。
用Cercon ht预烧结氧化锆块制作315个方形试件(10×10×4mm)。用氧化铝颗粒对氧化锆试件进行喷砂处理。这些试件被随机分为六个基于底漆的组:未涂抹底漆(NP)、Clearfil陶瓷底漆(C)、Panavia V5牙齿底漆(T)、M&C底漆(MC)、Monobond N(MN)和Z-PRIME plus(Z),然后再分为涂抹次数(1-4次)组(不包括NP)。每个试件用树脂水门汀粘结。使用万能试验机测量SBS。用体视显微镜检查脱粘表面。
采用双向方差分析对SBS进行分析。
每组中涂抹两次底漆的SBS最高,在T、MN和Z组中有显著差异。然而,MC组第二次涂抹时的SBS显著较低。所有组均观察到100%的粘结失败。
在本研究的局限性范围内,在粘结之前,喷砂处理的氧化锆表面应使用除MC之外的含磷酸盐底漆涂抹两次,以最大化氧化锆-树脂水门汀界面处的SBS。