Chen Xiao, Chhun Senghak, Xiang Jiqian, Tangjaidee Pipat, Peng Yaoyao, Quek Siew Young
Food Science, School of Chemical Sciences, The University of Auckland, Auckland 1010, New Zealand.
Enshi Tujia & Miao Autonomous Prefecture Academy of Agricultural Sciences, Enshi 445002, China.
Foods. 2021 Nov 24;10(12):2910. doi: 10.3390/foods10122910.
This study aimed to protect phenolic compounds of (Batal.) Iljinskaja () using a microencapsulation technique. Ethanol and aqueous extracts were prepared from leaves and microencapsulated via microfluidic-jet spray drying using three types of wall material: (1) maltodextrin (MD; 10-13, DE) alone; (2) MD:gum acacia (GA) of 1:1 ratio; (3) MD:GA of 1:3 ratio. The powders' physicochemical properties, microstructure, and phenolic profiles were investigated, emphasizing the retentions of the total and individual phenolic compounds and their antioxidant capacities () after spray drying. Results showed that all powders had good physical properties, including high solubilities (88.81 to 99.12%), low moisture contents (4.09 to 6.64%) and low water activities (0.11 to 0.19). The extract type used for encapsulation was significantly ( < 0.05) influenced the powder color, and more importantly the retention of total phenolic compounds (TPC) and . Overall, the ethanol extract powders showed higher TPC and values (50.93-63.94 mg gallic acid equivalents/g and 444.63-513.49 µM TE/g, respectively), while powders derived from the aqueous extract exhibited superior solubility, attractive color, and good retention of individual phenolic compounds after spray drying. The high-quality powders obtained in the current study will bring opportunities for use in functional food products with potential health benefits.
本研究旨在利用微胶囊技术保护(Batal.)Iljinskaja()的酚类化合物。从叶子中制备乙醇提取物和水提取物,并使用三种壁材通过微流控喷射干燥进行微胶囊化:(1)单独的麦芽糊精(MD;10 - 13,DE);(2)MD与阿拉伯胶(GA)比例为1:1;(3)MD与GA比例为1:3。研究了粉末的物理化学性质、微观结构和酚类特征,重点关注喷雾干燥后总酚类化合物和单个酚类化合物的保留情况及其抗氧化能力()。结果表明,所有粉末都具有良好的物理性质,包括高溶解度(88.81%至99.12%)、低水分含量(4.09%至6.64%)和低水分活度(0.11至0.19)。用于包封的提取物类型对粉末颜色有显著影响(<0.05),更重要的是对总酚类化合物(TPC)和的保留有影响。总体而言,乙醇提取物粉末显示出更高的TPC和值(分别为50.93 - 63.94毫克没食子酸当量/克和444.63 - 513.49微摩尔TE/克),而水提取物衍生的粉末在喷雾干燥后表现出优异的溶解度、吸引人的颜色和单个酚类化合物的良好保留。本研究中获得的高质量粉末将为用于具有潜在健康益处的功能性食品带来机会。