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基于二硅酸锂和硅酸锂并用氧化锆增强的用于计算机辅助设计/计算机辅助制造的玻璃陶瓷的抗弯强度

Flexural Strength of Vitreous Ceramics Based on Lithium Disilicate and Lithium Silicate Reinforced with Zirconia for CAD/CAM.

作者信息

Corado Hazel P R, da Silveira Pedro H P M, Ortega Vagner L, Ramos Guilherme G, Elias Carlos N

机构信息

Department of Materials Science, Instituto Militar de Engenharia-IME, Rio de Janeiro 22290-270, Brazil.

São Leopoldo Mandic University, Campinas 13045-755, Brazil.

出版信息

Int J Biomater. 2022 Feb 2;2022:5896511. doi: 10.1155/2022/5896511. eCollection 2022.

Abstract

The dental prosthesis market is rapidly evolving to meet patient and clinical demands. These new materials must have good flexural strength, toughness, aesthetic properties, and reliability in performance for structural applications. The present work aimed to compare the bending strength of 4 types of chairside lithium disilicate (LiSiO) glass-ceramics used for dental prosthesis and to analyze the influence of heat treatment on the transformation of lithium metasilicate (LiSiO) into lithium disilicate. The three-ball test for the biaxial flexion test (B3B) was used. Weibull statistical analysis was used, and it showed that samples with a higher percentage of zirconia have a greater tendency to fail. The flexion tests showed that the addition of more than 10% of zirconia reduced the flexural strength. The heat treatment process improves and provides greater mechanical strength. The XRD results indicated that the samples with the lowest percentage of zirconia exhibited greater crystallinity and corroborated the microstructural analysis. SEM analyses showed a greater amount and elongated crystals of lithium disilicate when comparing samples with a higher percentage of zirconia. Therefore, samples with lower zirconia showed greater flexural strength than samples with higher additions of zirconia.

摘要

牙科修复体市场正在迅速发展,以满足患者和临床需求。这些新材料必须具有良好的抗弯强度、韧性、美学性能以及在结构应用中的性能可靠性。本研究旨在比较4种用于牙科修复体的椅旁二硅酸锂(LiSiO)玻璃陶瓷的抗弯强度,并分析热处理对偏硅酸锂(LiSiO)向二硅酸锂转变的影响。采用双轴弯曲试验的三球试验(B3B)。使用了威布尔统计分析,结果表明氧化锆含量较高的样品有更大的失效倾向。弯曲试验表明,氧化锆添加量超过10%会降低抗弯强度。热处理过程可改善并提供更高的机械强度。X射线衍射结果表明,氧化锆含量最低的样品表现出更高的结晶度,这与微观结构分析结果相符。扫描电子显微镜分析表明,与氧化锆含量较高的样品相比,二硅酸锂晶体的数量更多且呈细长状。因此,氧化锆含量较低的样品比氧化锆添加量较高的样品表现出更高的抗弯强度。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/0dcf/8828337/ba3c403678c9/IJBM2022-5896511.001.jpg

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