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使用465纳米波长的SLA 3D打印技术制备和表征钛酸钡压电陶瓷

The Fabrication and Characterization of BaTiO Piezoceramics Using SLA 3D Printing at 465 nm Wavelength.

作者信息

Smirnov Andrey, Chugunov Svyatoslav, Kholodkova Anastasia, Isachenkov Maxim, Tikhonov Andrey, Dubinin Oleg, Shishkovsky Igor

机构信息

Skolkovo Institute of Science and Technology, 30/1 Bolshoi Boulevard, 121205 Moscow, Russia.

出版信息

Materials (Basel). 2022 Jan 26;15(3):960. doi: 10.3390/ma15030960.

DOI:10.3390/ma15030960
PMID:35160901
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC8838967/
Abstract

The additive manufacturing of BaTiO (BT) ceramics through stereolithography (SLA) 3D printing at 465 nm wavelength was demonstrated. After different milling times, different paste compositions with varied initial micron-sized powders were studied to find a composition suitable for 3D printing. The pastes were evaluated in terms of photopolymerization depth depending on the laser scanning speed. Furthermore, the microstructure and properties of the BT ceramic samples produced through SLA 3D printing were characterized and compared with those of ceramics fabricated through a conventional die semi-drying pressing method. Three-dimensional printed samples achieved relative densities over 0.95 and microhardness over 500 HV after sintering, nearly matching the relative density and microhardness attained by the pressed samples. Upon poling, the 3D-printed samples attained acceptable piezoelectric module d = 148 pC/N and dielectric constants over 2000. At near full density, BT piezoceramics were successfully fabricated through SLA 3D printing at 465 nm wavelength, achieving photopolymerization depth of more than 100 microns. This work paves the relatively low-cost way for 3D printing of piezoelectric ceramics using conventional micron-sized powders and high printed layer thickness.

摘要

展示了通过465nm波长的立体光刻（SLA）3D打印增材制造钛酸钡（BT）陶瓷的过程。在不同的研磨时间后，研究了具有不同初始微米级粉末的不同浆料组合物，以找到适合3D打印的组合物。根据激光扫描速度，对浆料的光聚合深度进行了评估。此外，对通过SLA 3D打印生产的BT陶瓷样品的微观结构和性能进行了表征，并与通过传统模压半干法制造的陶瓷进行了比较。三维打印样品在烧结后实现了超过0.95的相对密度和超过500 HV的显微硬度，几乎与压制样品的相对密度和显微硬度相匹配。极化后，3D打印样品获得了可接受的压电模量d = 148 pC/N和超过2000的介电常数。在接近全密度时，通过465nm波长的SLA 3D打印成功制造了BT压电陶瓷，实现了超过100微米的光聚合深度。这项工作为使用传统微米级粉末和高打印层厚度的压电陶瓷3D打印铺平了相对低成本的道路。

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