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通过多弧离子镀在纯钛表面沉积的不同厚度（钯/铁）涂层的磁性和生物相容性

Magnetic Properties and Biocompatibility of Different Thickness (Pd/Fe) Coatings Deposited on Pure Ti Surface via Multi Arc Ion Plating.

作者信息

Yang Zhijun, Li Junjie, Li Jinghua, Zhang Binbin, Li Jingxian, Sheng Shizhong, Ding Peng

机构信息

School of Mechanical and Electrical Engineering, Xinxiang University, Xinxiang 453003, China.

China Aviation Lithium Battery Technology Co., Ltd., Luoyang 471000, China.

出版信息

Materials (Basel). 2022 Feb 28;15(5):1831. doi: 10.3390/ma15051831.

DOI:10.3390/ma15051831
PMID:35269062
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC8911732/
Abstract

The different thickness (Fe/Pd) coatings were prepared by vacuum ion plating technology on a pure Ti substrate. The (Fe/Pd) coatings were magnetized using an MC-4000 high-pressure magnetizing machine. Then, the effect of the (Fe/Pd) coating thickness on the magnetic properties was studied. The surface and section morphology, composition, phase structure, magnetic properties, and biocompatibility of the (Fe/Pd) coatings were studied by scanning electron microscopy, X-ray diffraction, energy-dispersive X-ray spectroscopy, and CCTC-1 digital flux field measurement. The results showed that the (Fe/Pd) coatings were granular, smooth, and compact, without cracks. In addition the (Fe/Pd) coatings formed an L phase with a magnetic face-centered tetragonal-ordered structure after heat treatment. With the increase in the thickness of (FePd) coatings, the content of L FePd phase increased and the remanence increased. The remanence values of the Fe/Pd, (Fe/Pd), (Fe/Pd), and (Fe/Pd) magnetic coatings were 0.83 Gs, 5.52 Gs, 7.14 Gs, and 7.94 Gs, respectively. Additionally, the (Fe/Pd) magnetic coatings showed good blood compatibility and histocompatibility.

摘要

采用真空离子镀技术在纯钛基体上制备了不同厚度的（铁/钯）涂层。使用MC - 4000高压磁化机对（铁/钯）涂层进行磁化处理。然后，研究了（铁/钯）涂层厚度对磁性能的影响。通过扫描电子显微镜、X射线衍射、能量色散X射线光谱和CCTC - 1数字磁通场测量等手段，对（铁/钯）涂层的表面和截面形貌、成分、相结构、磁性能及生物相容性进行了研究。结果表明，（铁/钯）涂层呈颗粒状，表面光滑且致密，无裂纹。此外，（铁/钯）涂层在热处理后形成了具有磁性面心四方有序结构的L相。随着（铁钯）涂层厚度的增加，L - FePd相的含量增加，剩磁增大。铁/钯、（铁/钯）、（铁/钯）和（铁/钯）磁性涂层的剩磁值分别为0.83高斯、5.52高斯、7.14高斯和7.94高斯。此外，（铁/钯）磁性涂层表现出良好的血液相容性和组织相容性。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/8a19/8911732/5be96189df08/materials-15-01831-g011.jpg
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https://cdn.ncbi.nlm.nih.gov/pmc/blobs/8a19/8911732/5be96189df08/materials-15-01831-g011.jpg
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https://cdn.ncbi.nlm.nih.gov/pmc/blobs/8a19/8911732/c9a3d0d477b5/materials-15-01831-g006.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/8a19/8911732/8e6561192b19/materials-15-01831-g007a.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/8a19/8911732/fefdba4c9362/materials-15-01831-g008.jpg
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https://cdn.ncbi.nlm.nih.gov/pmc/blobs/8a19/8911732/82e17e0a45a0/materials-15-01831-g010.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/8a19/8911732/5be96189df08/materials-15-01831-g011.jpg

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