Politecnico di Milano, 20156 Milan, Italy.
School of Medicine, Nazarbayev University, Nur-Sultan 020000, Kazakhstan.
Sensors (Basel). 2022 Mar 15;22(6):2259. doi: 10.3390/s22062259.
This work presents an experimental investigation of the effect of chemical etching on the refractive index (RI) sensitivity of tilted fiber Bragg gratings (TFBGs). Hydrofluoric acid (HF) was used stepwise in order to reduce the optical fiber diameter from 125 µm to 13 µm. After each etching step, TFBGs were calibrated using two ranges of RI solutions: the first one with high RI variation (from 1.33679 RIU to 1.37078 RIU) and the second with low RI variation (from 1.34722 RIU to 1.34873 RIU). RI sensitivity was analyzed in terms of wavelength shift and intensity change of the grating resonances. The highest amplitude sensitivities obtained are 1008 dB/RIU for the high RI range and 8160 dB/RIU for the low RI range, corresponding to the unetched TFBG. The highest wavelength sensitivities are 38.8 nm/RIU for a fiber diameter of 100 µm for the high RI range, and 156 nm/RIU for a diameter of 40 µm for the small RI range. In addition, the effect of the etching process on the spectral intensity of the cladding modes, their wavelength separation and sensor linearity (R) were studied as well. As a result, an optimization of the etching process is provided, so that the best trade-off between sensitivity, intensity level, and fiber thickness can be obtained.
本工作研究了化学刻蚀对倾斜光纤布拉格光栅(TFBG)折射率(RI)灵敏度的影响。采用逐步的氢氟酸(HF)刻蚀方法,将光纤直径从 125μm 减小到 13μm。在每一步刻蚀之后,使用两个 RI 溶液范围对 TFBG 进行校准:第一个范围的 RI 变化较大(从 1.33679RIU 到 1.37078RIU),第二个范围的 RI 变化较小(从 1.34722RIU 到 1.34873RIU)。RI 灵敏度通过分析光栅共振的波长漂移和强度变化来评估。在高 RI 范围内获得的最高幅度灵敏度为 1008dB/RIU,在低 RI 范围内获得的最高幅度灵敏度为 8160dB/RIU,对应于未刻蚀的 TFBG。在高 RI 范围内,当光纤直径为 100μm 时,最高的波长灵敏度为 38.8nm/RIU,而在小 RI 范围内,当光纤直径为 40μm 时,最高的波长灵敏度为 156nm/RIU。此外,还研究了刻蚀过程对包层模的光谱强度、波长分离和传感器线性度(R)的影响。结果提供了刻蚀工艺的优化,从而可以在灵敏度、强度水平和光纤厚度之间获得最佳的折衷。