Yuan Zeye, Yu Kun, Li Longfei, Wang Gangquan, Zhang Kaihua, Liu Yufang
Henan Key Laboratory of Infrared Materials and Spectrum Measures and Applications, School of Physics, Henan Normal University, Xinxiang, Henan 453007, People's Republic of China.
Rev Sci Instrum. 2022 Apr 1;93(4):044902. doi: 10.1063/5.0073459.
A new apparatus simultaneously and rapidly measuring the sample radiation and the blackbody radiation by one detector without moving any experimental component is designed to measure the directional spectral emissivity of solid samples in a controlled environment. The effect of multiple reflections in the sample chamber on the measurement result is evaluated. The temperature distribution of the sample surface is measured by using a thermal imager. In order to validate the experimental apparatus, the directional spectral emissivity of silicon is measured in a nitrogen environment and that of iron is measured in vacuum, and the normal spectral emissivity of pure copper is measured during the oxidation process. Good agreement between the measured results and the reported data proves the reliability of the designed apparatus. The expanded uncertainty of the measurement system is estimated to be less than 5.3% when the emission angle is 86°.
设计了一种新装置,可通过一个探测器同时快速测量样品辐射和黑体辐射,无需移动任何实验部件,用于在可控环境中测量固体样品的定向光谱发射率。评估了样品室中多次反射对测量结果的影响。使用热成像仪测量样品表面的温度分布。为了验证该实验装置,在氮气环境中测量了硅的定向光谱发射率,在真空中测量了铁的定向光谱发射率,并在氧化过程中测量了纯铜的法向光谱发射率。测量结果与报道数据之间的良好一致性证明了所设计装置的可靠性。当发射角为86°时,测量系统的扩展不确定度估计小于5.3%。