Li Longfei, Wang Fayu, Gao Jiaying, Yu Kun, Wang Lan, Liu Yufang
Henan Key Laboratory of Infrared Spectrum Measures and Applications, School of Physics, Henan Normal University, Xinxiang 453007, China.
Sensors (Basel). 2024 Sep 11;24(18):5906. doi: 10.3390/s24185906.
Accurate measurement of the infrared spectral emissivity of nickel-based alloys is significant for applications in aerospace. The low thermal conductivity of these alloys limits the accuracy of direct emissivity measurement, especially during the oxidation process. To improve measurement accuracy, a surface temperature correction method based on two thermocouples was proposed to eliminate the effect of thermal conductivity changes on emissivity measurement. By using this method, the infrared spectral emissivity of Inconel 601, Inconel 625, and Inconel 718 alloys was accurately measured during the oxidation process, with a temperature range of 673-873 K, a wavelength range of 3-20 μm, and a zenith angle range of 0-80°. The results show that the emissivity of the three alloys is similar in value and variation law; the emissivity of Inconel 718 is slightly less than that of Inconel 601 and Inconel 625; and the spectral emissivity of the three alloys strongly increases in the first hour, whereafter it grows gradually with the increase in oxidation time. Finally, Inconel 601 has a lower emissivity growth rate, which illustrates that it possesses stronger oxidation resistance and thermal stability. The maximum relative uncertainty of the emissivity measurement of the three alloys does not exceed 2.6%, except for the atmospheric absorption wavebands.
准确测量镍基合金的红外光谱发射率对航空航天应用具有重要意义。这些合金的低导热率限制了直接发射率测量的准确性,尤其是在氧化过程中。为提高测量精度,提出了一种基于两个热电偶的表面温度校正方法,以消除导热率变化对发射率测量的影响。采用该方法,在673 - 873 K的温度范围、3 - 20μm的波长范围和0 - 80°的天顶角范围内,准确测量了Inconel 601、Inconel 625和Inconel 718合金在氧化过程中的红外光谱发射率。结果表明,三种合金的发射率在数值和变化规律上相似;Inconel 718的发射率略低于Inconel 601和Inconel 625;三种合金的光谱发射率在最初一小时内大幅增加,此后随氧化时间的增加而逐渐增长。最后,Inconel 601具有较低的发射率增长率,这表明它具有更强的抗氧化性和热稳定性。除大气吸收波段外,三种合金发射率测量的最大相对不确定度不超过2.6%。