一种在无溶剂超声条件下以MIL-53(Al)为催化剂合成吡咯的温和高效方法。
A mild and efficient method for the synthesis of pyrroles using MIL-53(Al) as a catalyst under solvent-free sonication.
作者信息
Nguyen Hai Truong, Thuy Nguyen Linh Ho, Le Hoang Doan Tan, Tran Phuong Hoang
机构信息
Faculty of Chemistry, University of Science, Vietnam National University - Ho Chi Minh City 721337 Vietnam
Center for Innovative Materials and Architectures, Vietnam National University - Ho Chi Minh City 721337 Vietnam
出版信息
RSC Adv. 2019 Mar 19;9(16):9093-9098. doi: 10.1039/c9ra01071h. eCollection 2019 Mar 15.
A highly efficient method for the synthesis of pyrroles using MIL-53(Al) as a catalyst has been developed under solvent-free sonication. This reaction has a broad substrate scope and high yields were obtained within a short reaction time. Remarkably, no additional additives and volatile organic solvent are required for this method and the MIL-53(Al) could be recovered and reused several times without significant drop-off in catalytic activity.
已开发出一种在无溶剂超声处理条件下使用MIL-53(Al)作为催化剂合成吡咯的高效方法。该反应具有广泛的底物范围，并且在短反应时间内可获得高产率。值得注意的是，该方法无需额外的添加剂和挥发性有机溶剂，并且MIL-53(Al)可以回收并重复使用几次，而催化活性不会显著下降。
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