Karaluka Valerija, Murata Kengo, Masuda Shinto, Shiramatsu Yuto, Kawamoto Takuji, Hailes Helen C, Sheppard Tom D, Kamimura Akio
Department of Applied Chemistry, Yamaguchi University Ube 755-8611 Japan
Department of Chemistry, University College London 20 Gordon Street London WC1H 0AJ UK.
RSC Adv. 2018 Jun 20;8(40):22617-22624. doi: 10.1039/c8ra03895c. eCollection 2018 Jun 19.
A sustainable synthetic procedure to convert furfural hydrazones into functionalised phthalimides was developed. The reaction was performed in a microwave using a hydrophilic ionic liquid, [bmim][Cl], as the solvent which could be readily recovered by a simple extraction. The ionic liquid was successfully recycled with no significant loss in product yields.
开发了一种将糠醛腙转化为功能化邻苯二甲酰亚胺的可持续合成方法。该反应在微波条件下使用亲水性离子液体[bmim][Cl]作为溶剂进行，通过简单萃取即可轻松回收该溶剂。离子液体成功实现了循环利用，产品收率没有显著损失。
