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水热老化后全瓷热压和CAD/CAM修复体的断口分析及显微硬度评估

Fractographic and Microhardness Evaluation of All-Ceramic Hot-Pressed and CAD/CAM Restorations after Hydrothermal Aging.

作者信息

Vasiliu Roxana Diana, Uțu Ion-Dragoș, Rusu Lucian, Boloș Adrian, Porojan Liliana

机构信息

Center for Advanced Technologies in Dental Prosthodontics, Department of Dental Prostheses Technology (Dental Technology), Faculty of Dental Medicine, "Victor Babeș" University of Medicine and Pharmacy Timișoara, Eftimie Murgu Sq. No. 2, 300041 Timișoara, Romania.

Departament of Materials Engineering and Fabrication, University of Politehnică Timişoara, Bd. Mihai Viteazul nr.1, 300222 Timişoara, Romania.

出版信息

Materials (Basel). 2022 Jun 3;15(11):3987. doi: 10.3390/ma15113987.

Abstract

All-ceramic dental restorations have great advantages, such as highly esthetical properties, a less complex fabrication, and a similar abrasion resistance to enamel. Despite these advantages, ceramic materials are more prone to fracture due to their brittle microstructure. The main aim of this in vitro study was to determine the difference in hot-pressed and milled glass-ceramic mechanical properties such as fracture resistance and microhardness (VHN). Four types of ceramics, two hot-pressed and two milled, feldspathic glass-ceramics and zirconia-reinforced glass-ceramics were selected in this study and tested using the static loading test and Vicker’s testing. Hydrothermal aging, consisting of different baths with temperatures between 5 degrees Celsius and 55 degrees Celsius, was chosen as the in vitro aging method. Statistical analyses are performed using SPSS Statistics software at a significance level of p < 0.05. Micro-hardness values decrease after hydrothermal aging. The static loading test reveals a significant difference between the feldspathic hot-pressed glass-ceramic, which fractures at lower forces, and milled zirconia-reinforced lithium silicate glass-ceramic, which fractures at greater forces (N). Fractographic analysis of the fractured fragments resulted in the static loading test revealing different surface features about the crack origins and propagations under a stereomicroscope.

摘要

全瓷牙科修复体具有很大的优势,如高度美观的性能、制作过程不太复杂以及与牙釉质相似的耐磨性。尽管有这些优点,但陶瓷材料由于其脆性微观结构更容易断裂。这项体外研究的主要目的是确定热压和研磨玻璃陶瓷的机械性能差异,如抗断裂性和显微硬度(维氏硬度)。本研究选择了四种类型的陶瓷,两种热压的和两种研磨的,分别是长石质玻璃陶瓷和氧化锆增强玻璃陶瓷,并使用静态加载试验和维氏试验进行测试。选择在5摄氏度至55摄氏度之间不同温度的水浴进行水热老化作为体外老化方法。使用SPSS Statistics软件进行统计分析,显著性水平为p < 0.05。水热老化后显微硬度值降低。静态加载试验显示,在较低力作用下断裂的长石质热压玻璃陶瓷与在较大力(牛顿)作用下断裂的研磨氧化锆增强硅酸锂玻璃陶瓷之间存在显著差异。对断裂碎片的断口分析通过静态加载试验在体视显微镜下揭示了裂纹起源和扩展的不同表面特征。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2b88/9182156/7874bfab3af1/materials-15-03987-g001.jpg

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