Abdullah Johar Amin Ahmed, Jiménez-Rosado Mercedes, Perez-Puyana Víctor, Guerrero Antonio, Romero Alberto
Departamento de Ingeniería Química, Escuela Politécnica Superior, Universidad de Sevilla, 41011 Sevilla, Spain.
Departamento de Ingeniería Química, Facultad de Química, Universidad de Sevilla, 41012 Sevilla, Spain.
Nanomaterials (Basel). 2022 Jul 17;12(14):2449. doi: 10.3390/nano12142449.
Iron oxide nanoparticles (FeO-NPs) are currently being applied in numerous high-tech sectors, such as in chemical sectors for catalysis and in the medical sector for drug delivery systems and antimicrobial purposes, due to their specific, unique and magnetic properties. Nevertheless, their synthesis is under continuous investigation, as physicochemical methods are considered expensive and require toxic solvents. Thus, green nanotechnology has shown considerable promise in the eco-biogenesis of nanoparticles. In the current study, FeO-NPs were synthesized by two different methods: via green synthesis through the use of polyphenols, which were extracted from L.; and via chemical synthesis, in which the reducing agent was a chemical (NaOH), and iron chloride was used as a precursor. Thus, polyphenol extraction and its ability to produce nanoparticles were evaluated based on the drying temperature used during the L. recollection, as well as the extraction solvent used. The results highlight the potential of polyphenols present in L. for the sustainable manufacture of FeO-NPs. Finally, green and chemical syntheses were compared on the basis of physicochemical characteristics and functional properties.
氧化铁纳米颗粒(FeO-NPs)由于其特定、独特的磁性特性,目前正应用于众多高科技领域,如化学领域的催化以及医学领域的药物递送系统和抗菌用途。然而,由于物理化学方法被认为成本高昂且需要使用有毒溶剂,其合成仍在持续研究中。因此,绿色纳米技术在纳米颗粒的生态生物合成方面显示出了巨大的潜力。在本研究中,通过两种不同方法合成了FeO-NPs:一种是通过使用从[植物名称未完整给出]中提取的多酚进行绿色合成;另一种是化学合成,其中还原剂为化学物质(NaOH),并使用氯化铁作为前驱体。因此,基于[植物名称未完整给出]回收过程中使用的干燥温度以及所使用的提取溶剂,对多酚提取及其产生纳米颗粒的能力进行了评估。结果突出了[植物名称未完整给出]中存在的多酚在可持续制造FeO-NPs方面的潜力。最后,基于物理化学特性和功能特性对绿色合成和化学合成进行了比较。