Department of Electronic and Photonic Metrology, Wroclaw University of Science and Technology, 50-317 Wroclaw, Poland.
Sensors (Basel). 2022 Nov 5;22(21):8525. doi: 10.3390/s22218525.
A low electromagnetic interference (EMI), precision temperature control system for sensitive piezoelectric sensors stabilization and their thermal characteristics research was proposed. Quartz crystal microbalance (QCM) was chosen as the device to be tested. Recently, QCMs found use in many fields of study such as biology, chemistry, and aerospace. They often operate in harsh environments and are exposed to many external factors including temperature fluctuations, to which QCMs are highly susceptible. Such disturbances can cause undesirable resonant frequency shifts resulting in measurement errors that are difficult to eliminate. The proposed solution enables measurements of QCMs thermal characteristics, effectiveness evaluation of temperature compensation methods, and testing of the frequency stability. As a part of the developed solution, two independent temperature regulators were used: first to maintain the QCM crystal at desired temperature, and second to keep the QCM oscillator circuit at fixed temperature. The single regulator consists of a thermoelectric module (TEC) used for both heating and cooling. Two considered TEC driving methods were compared in terms of EMI and their impact on the QCM signal quality. The proposed system was examined for its temperature stabilization capability showing high stability of 11 mK for one hour and the setpoint accuracy of ±15 mK in the full temperature range.
提出了一种低电磁干扰(EMI)、精密温度控制系统,用于敏感压电传感器的稳定及其热特性研究。选择石英晶体微天平(QCM)作为待测试的器件。最近,QCM 在生物学、化学和航空航天等许多研究领域得到了应用。它们通常在恶劣的环境中工作,并受到许多外部因素的影响,包括温度波动,QCM 对此非常敏感。这种干扰会导致不理想的共振频率偏移,从而导致难以消除的测量误差。所提出的解决方案能够测量 QCM 的热特性、评估温度补偿方法的有效性以及测试频率稳定性。作为开发解决方案的一部分,使用了两个独立的温度调节器:第一个用于将 QCM 晶体保持在所需温度,第二个用于将 QCM 振荡器电路保持在固定温度。单个调节器由用于加热和冷却的热电模块(TEC)组成。比较了两种考虑的 TEC 驱动方法在 EMI 及其对 QCM 信号质量的影响方面的性能。所提出的系统经过温度稳定能力的测试,在一个小时内表现出 11 mK 的高稳定性,在整个温度范围内的设定点精度为±15 mK。