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多糖作为合成 MgO 的绿色燃料:特性分析及抗菌活性评估。

Polysaccharides as Green Fuels for the Synthesis of MgO: Characterization and Evaluation of Antimicrobial Activities.

机构信息

Departamento de Química, Universidade Estadual do Centro-Oeste, Guarapuava 85040-080, Brazil.

Chimie des Interactions Plasma-Surface (ChIPS), Research Institute for Materials Science and Engineering, University of Mons, 7000 Mons, Belgium.

出版信息

Molecules. 2022 Dec 24;28(1):142. doi: 10.3390/molecules28010142.

Abstract

The synthesis of structured MgO is reported using feedstock starch (route I), citrus pectin (route II), and (route III) leaf, which are suitable for use as green fuels due to their abundance, low cost, and non-toxicity. The oxides formed showed high porosity and were evaluated as antimicrobial agents. The samples were characterized by energy-dispersive X-ray fluorescence (EDXRF), X-ray diffraction (XRD), Fourier-transform infrared spectroscopy (FTIR), and scanning electron microscopy (SEM). The crystalline periclase monophase of the MgO was identified for all samples. The SEM analyses show that the sample morphology depends on the organic fuel used during the synthesis. The antibacterial activity of the MgO-St (starch), MgO-CP (citrus pectin), and MgO-Av ( oxides was evaluated against pathogens (ATCC 6538P) and (ATCC 8739). Antifungal activity was also studied against (ATCC 64548). The studies were carried out using the qualitative agar disk diffusion method and quantitative minimum inhibitory concentration (MIC) tests. The MIC of each sample showed the same inhibitory concentration of 400 µg. mL for the studied microorganisms. The formation of inhibition zones and the MIC values in the antimicrobial analysis indicate the effective antimicrobial activity of the samples against the test microorganisms.

摘要

采用富含淀粉(路线 I)、柑橘果胶(路线 II)和 (路线 III)叶的原料合成了结构可控的氧化镁,由于其丰富、廉价和无毒,这些原料适合用作绿色燃料。所形成的氧化物表现出高孔隙率,并被评估为抗菌剂。通过能量色散 X 射线荧光(EDXRF)、X 射线衍射(XRD)、傅里叶变换红外光谱(FTIR)和扫描电子显微镜(SEM)对样品进行了表征。所有样品均鉴定出结晶氧化镁的单相尖晶石。SEM 分析表明,样品形态取决于合成过程中使用的有机燃料。使用定性琼脂盘扩散法和定量最小抑菌浓度(MIC)测试评估了 MgO-St(淀粉)、MgO-CP(柑橘果胶)和 MgO-Av( )对病原菌 (ATCC 6538P)和 (ATCC 8739)的抗菌活性。还研究了对 (ATCC 64548)的抗真菌活性。研究采用定性琼脂盘扩散法和定量最小抑菌浓度(MIC)测试进行。每个样品的 MIC 均显示出对研究微生物相同的抑制浓度 400 µg。mL。抑菌分析中的抑菌圈形成和 MIC 值表明,这些样品对测试微生物具有有效的抗菌活性。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d86b/9822341/5e943957c38c/molecules-28-00142-g001.jpg

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