School of Mechanical and Manufacturing Engineering, UNSW Sydney, Sydney, NSW, 2052, Australia.
ARC Training Centre for Automated Manufacture of Advanced Composites, UNSW Sydney, Sydney, NSW, 2052, Australia.
Sci Rep. 2023 Jan 25;13(1):1397. doi: 10.1038/s41598-023-28645-6.
Fibre-reinforced biocomposites usage has gained prominence over the past decade. Although higher fracture toughness was observed when fibres were added to biocomposites, material degradation could occur due to filler and fibre content intolerance in the biocomposite matrix. Optimisation of resin-fibre-filler ratios helps in increasing the tribological performance of high load-bearing applications. However, the tribological performance is less understood due to limited in-vitro studies on the effect of fibre microstructures. A comprehensive investigation of the reciprocating and rotary wear behaviour of different compositions was carried out by varying fibre (0%, 5%, 10% and 15%) to particulate filler (40%, 45%, 50%, and 55%) weight fractions. The investigation aimed to identify the optimal composition of fibre-reinforced biocomposites based on the in-vitro ball-on-disc reciprocating and rotary wear tests in the presence of modified Fusayama solution. The cross-sectional areas of wear tracks were analysed using laser microscopy and scanning electron microscopy techniques to assess the surface morphology and subsurface damage of the wear tracks on biocomposites and the antagonist. The numerical results were statistically analysed using two-way ANOVA followed by a posthoc Tukey's test (p = 0.05). The results showed a combination of adhesive, abrasive and fatigue wear for all the tested Groups. The friction coefficient had a longer transient period for the 5 wt% and 10 wt% Groups. Based on the surface roughness, coefficient of friction, SEMs, specific wear rate, and ease of manufacturing, the threshold limit for fibre loading was found to be 10 wt%. The rotary test had a considerably lower specific wear rate compared to the reciprocating test. Fibre weight fraction was found to be the influencing factor of the abrasive wear behaviour compared to fibre length for the tested Groups.
在过去十年中,纤维增强生物复合材料的使用得到了重视。虽然在向生物复合材料中添加纤维时观察到了更高的断裂韧性,但由于复合材料基体中填料和纤维含量不兼容,可能会发生材料降解。优化树脂-纤维-填料的比例有助于提高高承载应用的摩擦学性能。然而,由于对纤维微观结构的影响的体外研究有限,因此对其摩擦学性能的了解较少。通过改变纤维(0%、5%、10%和 15%)和颗粒状填料(40%、45%、50%和 55%)的重量分数,对不同成分的往复和旋转磨损行为进行了全面研究。研究旨在通过在改良 Fusayama 溶液存在的情况下进行体外球盘往复和旋转磨损试验,根据纤维增强生物复合材料的最佳组成。使用激光显微镜和扫描电子显微镜技术分析磨损轨道的横截面面积,以评估生物复合材料和对磨件上磨损轨道的表面形貌和次表面损伤。使用双因素方差分析(ANOVA)和事后 Tukey 检验(p = 0.05)对数值结果进行了统计分析。结果表明,所有测试组都存在粘着、磨料和疲劳磨损的组合。对于 5 wt%和 10 wt%组,摩擦系数的过渡阶段较长。基于表面粗糙度、摩擦系数、SEM、比磨损率和易于制造性,发现纤维负载的阈值限制为 10 wt%。与往复试验相比,旋转试验的比磨损率低得多。与纤维长度相比,纤维重量分数是影响测试组的磨料磨损行为的因素。