Lassila Lippo, Garoushi Sufyan, Vallittu Pekka K, Säilynoja Eija
Department of Biomaterials Science and Turku Clinical Biomaterial Center -TCBC Institute of Dentistry, University of Turku, Turku, Finland.
Department of Biomaterials Science and Turku Clinical Biomaterial Center -TCBC Institute of Dentistry, University of Turku, Turku, Finland.
J Mech Behav Biomed Mater. 2016 Jul;60:331-338. doi: 10.1016/j.jmbbm.2016.01.036. Epub 2016 Feb 16.
The purpose of this study was to investigate the reinforcing effect of discontinuous glass fiber fillers with different length scales on fracture toughness and flexural properties of dental composite.
Experimental fiber reinforced composite (Exp-FRC) was prepared by mixing 27wt% of discontinuous E-glass fibers having two different length scales (micrometer and millimeter) with various weight ratios (1:1, 2:1, 1:0 respectively) to the 23wt% of dimethacrylate based resin matrix and then 50wt% of silane treated silica filler were added gradually using high speed mixing machine. As control, commercial FRC and conventional posterior composites were used (everX Posterior, Alert, and Filtek Superme). Fracture toughness, work of fracture, flexural strength, and flexural modulus were determined for each composite material following ISO standards. The specimens (n=6) were dry stored (37°C for 2 days) before they were tested. Scanning electron microscopy was used to evaluate the microstructure of the experimental FRC composites. The results were statistically analyzed using ANOVA followed by post-hoc Tukey׳s test. Level of significance was set at 0.05.
ANOVA revealed that experimental composites reinforced with different fiber length scales (hybrid Exp-FRC) had statistically significantly higher mechanical performance of fracture toughness (4.7MPam(1/2)) and flexural strength (155MPa) (p<0.05) compared to other tested composites.
The use of different length scales of discontinues fiber fillers (hybrid) with polymer matrix yielded improved mechanical performance compared to commercial FRC and conventional posterior composites.
本研究旨在探讨不同长度尺度的间断玻璃纤维填料对牙科复合材料断裂韧性和弯曲性能的增强效果。
通过将27wt%具有两种不同长度尺度(微米和毫米)的间断E玻璃纤维按不同重量比(分别为1:1、2:1、1:0)与23wt%的二甲基丙烯酸酯基树脂基体混合,制备实验性纤维增强复合材料(Exp-FRC),然后使用高速混合机逐渐添加50wt%经硅烷处理的二氧化硅填料。作为对照,使用了市售纤维增强复合材料和传统后牙复合材料(everX Posterior、Alert和Filtek Superme)。按照ISO标准测定每种复合材料的断裂韧性、断裂功、弯曲强度和弯曲模量。在测试前,将试样(n = 6)干燥储存(37°C,2天)。使用扫描电子显微镜评估实验性纤维增强复合材料的微观结构。结果采用方差分析(ANOVA),随后进行事后Tukey检验进行统计分析。显著性水平设定为0.05。
方差分析显示,与其他测试复合材料相比,用不同长度尺度纤维增强的实验性复合材料(混合Exp-FRC)在断裂韧性(4.7MPam(1/2))和弯曲强度(155MPa)方面具有统计学显著更高的力学性能(p<0.05)。
与市售纤维增强复合材料和传统后牙复合材料相比,将不同长度尺度的间断纤维填料(混合)与聚合物基体一起使用可提高力学性能。