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微波诱导溶液燃烧法合成金属氧化物纳米材料综述

A review on the synthesis of metal oxide nanomaterials by microwave induced solution combustion.

作者信息

Yin Ziyang, Li Si, Li Xiang, Shi Wuyang, Liu Wei, Gao Zhengxia, Tao Mengya, Ma Chengliang, Liu Yuan

机构信息

Henan Key Laboratory of High Temperature Functional Ceramics, School of Material Science and Engineering, Zhengzhou University 75 Daxue Road Zhengzhou 450052 China

出版信息

RSC Adv. 2023 Jan 20;13(5):3265-3277. doi: 10.1039/d2ra07936d. eCollection 2023 Jan 18.

DOI:10.1039/d2ra07936d
PMID:36756450
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC9854637/
Abstract

With the increasing awareness of environmental protection and health, the preparation of metal oxide nanomaterials by environmentally friendly methods is favored by more and more researchers both at home and abroad. The preparation of metal oxide nanomaterials by a microwave-induced solution combustion synthesis method can significantly reduce the reaction time, energy consumption, and the use of toxic chemicals, which is an energy-saving, environmentally friendly method for nanomaterials synthesis. In addition, the microwave-induced solution combustion synthesis (MISCS) method has many advantages such as fast reaction speed, high selectivity, small product size, and homogeneous composition. This paper briefly describes the mechanism of the MISCS and its advantages in the synthesis of metal oxide nanomaterials, the related studies on microwave-induced solution combustion synthesis of metal oxide nanomaterials, and the effects of process parameters on the microstructure and properties of metal oxide nanomaterials synthesized by MISCS. Furthermore, some technical difficulties facing the synthesis of metal oxide nanomaterials by MISCS are summarized, and the future direction has also been prospected.

摘要

随着环境保护和健康意识的不断提高,采用环境友好型方法制备金属氧化物纳米材料受到了越来越多国内外研究者的青睐。通过微波诱导溶液燃烧合成法制备金属氧化物纳米材料能够显著缩短反应时间、降低能耗并减少有毒化学品的使用,这是一种用于纳米材料合成的节能、环境友好型方法。此外,微波诱导溶液燃烧合成(MISCS)法具有反应速度快、选择性高、产物尺寸小和成分均匀等诸多优点。本文简要介绍了MISCS的机理及其在金属氧化物纳米材料合成中的优势、微波诱导溶液燃烧合成金属氧化物纳米材料的相关研究,以及工艺参数对通过MISCS合成的金属氧化物纳米材料微观结构和性能的影响。此外,总结了MISCS法合成金属氧化物纳米材料面临的一些技术难题,并对未来发展方向进行了展望。

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