以 TfO 作为三氟甲氧基化试剂 CFSOCF 的 CF 源。
TfO as a CF Source for the Synthesis of Trifluoromethoxylation Reagent CFSOCF.
机构信息
Hubei Key Laboratory of Pollutant Analysis and Reuse Technology, College of Chemistry and Chemical Engineering, Hubei Normal University, Huangshi 435002, China.
Key Laboratory of Organofluorine Chemistry, Shanghai Institute of Organic Chemistry, University of Chinese Academy of Sciences, Chinese Academy of Sciences, 345 Lingling Road, Shanghai 200032, China.
出版信息
J Org Chem. 2023 Mar 3;88(5):3346-3352. doi: 10.1021/acs.joc.2c03018. Epub 2023 Feb 10.
PMID:36763542
Abstract
Described herein is the convenient synthesis of an efficient trifluoromethoxylation reagent, CFSOCF, by using cheap and widely available reagents and without the need of any tedious column chromatography purification procedure.
摘要
本文介绍了一种方便合成高效三氟甲氧基化试剂 CFSOCF 的方法，该方法使用廉价且广泛可用的试剂，无需繁琐的柱层析纯化步骤。
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